본문 바로가기
KERD
논문KCI 미등재

Technical Overview on the Electron Backscattered Diffraction Sample Preparation

2

조회

0

다운로드

0

인용

0

참고문헌

키워드

주제분류자연과학일반

초록

A technical overview on the various sample preparation methods for electron backscattered diffraction (EBSD) analysis is carried out. The mechanical polishing with colloidal silica f nish, electro-chemical polishing, dual layer coating and ion beam milling are introduced for the common sample preparation methods for EBSD observation and some issues that are frequently neglected by the common EBSD users but should be considered to get a reliable EBSD data are discussed. This overview would be especially helpful to the people who know what EBSD technique is but do not get a reliable EBSD data because of diff culties in sample preparation.

Abstract

A technical overview on the various sample preparation methods for electron backscattered diffraction (EBSD) analysis is carried out. The mechanical polishing with colloidal silica f nish, electro-chemical polishing, dual layer coating and ion beam milling are introduced for the common sample preparation methods for EBSD observation and some issues that are frequently neglected by the common EBSD users but should be considered to get a reliable EBSD data are discussed. This overview would be especially helpful to the people who know what EBSD technique is but do not get a reliable EBSD data because of diff culties in sample preparation.

참고문헌 (9)

  1. Humphreys F J, "Determination of microtexture by EBSD at high spatial resolution in a FEGSEM", Proceedings of ICOTOM-12, pp.74~78 (1999), NRC Research Press
  2. Jung S J, "Hardening of Bi–Te based alloys by dispersing B4C nanoparticles", Acta Mater, 97, pp.68~74 (2015)
  3. Kim D I, "Characterization of crystallographic properties of SMC poly Si using electron backscattered diffraction", J. Microsc, 215, pp.121~126 (2004)
  4. Kim D I, "Microtexture measurement of copper damascene line with EBSD", Mater. Sci. Forum, 408-412, pp.529~534 (2002)
  5. Kim J H, "Investigation into the high temperature oxidation of Cu-bearing austenitic stainless steel using simultaneous electron backscatter diffraction-energy dispersive spectroscopy analysis", Corros. Sci, 77, pp.397~402 (2013)
  6. Lassen N C K, "Automated Determination of Crystal Orientations from Electron Backscattering Patterns", pp.1994
  7. Muppidi T, "Barrier layer, geometry and alloying effects on the microstructure and texture of electroplated copper thin films and damascene lines", Thin Solid Films, 471, pp.63~70 (2005)
  8. Schwartz A J, "Electron Backscatter Diffraction in Materials Science" (2010), Springer Science & Business Media
  9. Venables J A, "Electron back-scattering patterns:a new technique for obtaining crystallographic information in the scanning electron microscope", Phil. Mag, 27, pp.1193~1200 (1973)

관련 논문AI추천

이 간행물의 다른 논문 (12건)