Structural and component characterization of the B4C neutron conversion layer deposited by magnetron sputtering
2
조회
0
다운로드
0
인용
0
참고문헌
키워드
초록
Neutron conversion detectors that use 10B-enriched boron carbide are feasible alternatives to 3 He-based detectors. We prepared boron carbide films at micron-scale thickness using direct-current magnetron sputtering. The structural characteristics of natural B4C films, including density, roughness, crystallization, and purity, were analyzed using grazing incidence X-ray reflectivity, X-ray diffraction, X-ray photoelectron spectroscopy, time-of-flight secondary ion mass spectrometry, and scanning electron microscopy. A beam profile test was conducted to verify the practicality of the 10B-enriched B4C neutron conversion layer. A clear profile indicated the high quality of the neutron conversion of the boron carbide layer.
Abstract
Neutron conversion detectors that use 10B-enriched boron carbide are feasible alternatives to 3 He-based detectors. We prepared boron carbide films at micron-scale thickness using direct-current magnetron sputtering. The structural characteristics of natural B4C films, including density, roughness, crystallization, and purity, were analyzed using grazing incidence X-ray reflectivity, X-ray diffraction, X-ray photoelectron spectroscopy, time-of-flight secondary ion mass spectrometry, and scanning electron microscopy. A beam profile test was conducted to verify the practicality of the 10B-enriched B4C neutron conversion layer. A clear profile indicated the high quality of the neutron conversion of the boron carbide layer.
참고문헌 (17)
- Zhong Zhang, "Stress evolution in B4C and Cr mono-layer and B4C", Cr multilayer films with variable layer thickness for neutron detectors, 2013, pp.531, 302~305[DOI]
- Jeffrey L. Lacy, "Boron-coated straws as a replacement for 3He-based neutron detectors", Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 652(1), pp.359~363 (2011), Elsevier BV[DOI]
- Adrian Cho, "Helium-3 Shortage Could Put Freeze On Low-Temperature Research", Science, 326(5954), pp.778~779 (2009), American Association for the Advancement of Science (AAAS)[DOI]
- Karl Zeitelhack, "Search for alternative techniques to helium-3 based detectors for neutron scattering applications", Neutron News, 23(4), pp.10~13 (2012), Informa UK Limited[DOI]
- F. Piscitelli, "Neutron reflectometry on highly absorbing films and its application to (B4C)-B-10-based neutron detectors", Proceedings of the Royal Society A: Mathematical, Physical and Engineering Sciences, 472(2185), pp.20150711~ (2016), The Royal Society[DOI]
- M. Henske, "The 10B based Jalousie neutron detector – An alternative for 3He filled position sensitive counter tubes", Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 686, pp.151~155 (2012), Elsevier BV[DOI]
- N. Hong, "An Exploration of Neutron Detection in Semiconducting Boron Carbide", pp.2012
- Carina Höglund, "B4C thin films for neutron detection", Journal of Applied Physics, 111(10) (2012), AIP Publishing[DOI]
- Susann Schmidt, "Low-temperature growth of boron carbide coatings by direct current magnetron sputtering and high-power impulse magnetron sputtering", Journal of Materials Science, 51(23), pp.10418~10428 (2016), Springer Science and Business Media LLC[DOI]
- Henrik Pedersen, "Low Temperature CVD of Thin, Amorphous Boron‐Carbon Films for Neutron Detectors", Chemical Vapor Deposition, 18(7-9), pp.221~224 (2012), Wiley[DOI]
- G. Nowak, "Boron carbide coatings for neutron detection probed by x-rays, ions, and neutrons to determine thin film quality", Journal of Applied Physics, 117(3) (2015), AIP Publishing[DOI]
- T. Bigault, "10B multi-grid proportional gas counters for large area thermal neutron detectors", Neutron News, 23(4), pp.20~25 (2012), Informa UK Limited[DOI]
- I. Stefanescu, "Development of a novel macrostructured cathode for large-area neutron detectors based on the 10B-containing solid converter", Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 727, pp.109~125 (2013), Elsevier BV[DOI]
- Hesheng Chen, "China's first pulsed neutron source", Nature Materials, 15(7), pp.689~691 (2016), Springer Science and Business Media LLC[DOI]
- L. G. Parratt, "Surface Studies of Solids by Total Reflection of X-Rays", Physical Review, 95(2), pp.359~369 (1954), American Physical Society (APS)[DOI]
- Mei-Ling Wu, "Process–property relationship of boron carbide thin films by magnetron sputtering", Thin Solid Films, 449(1-2), pp.120~124 (2004), Elsevier BV[DOI]
- Zhou Jianrong, "A novel ceramic GEM used for neutron detection", Nuclear Engineering and Technology, 52(6), pp.1277~1281 (2020), 한국원자력학회[DOI]
