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액체 질소의 흐름 조절을 통한 저온 정밀 온도 제어

Precise temperature control by adjusting flow of liquid nitrogen

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주제분류공학일반

초록

We devised a method to control the temperature of a liquid bath as low as –100oC using the duty cycle control of a solenoid valve. The solenoid valve controls the flow of liquid nitrogen that we used as a cryogen in this system. By controlling the duty cycle of a solenoid valve using feedback from the measured temperature of the liquid bath, we were able to achieve temperature stability within ±19 mK around –100oC. We also demonstrated that by taking average values of the temperature readings for sequence of measurements from more than one thermometer, it is possible to use this system for the calibration of thermometers within 3 mK. This system and the control method can be used for the precise temperature control in the range between 0oC and –100oC, where commercially available precision baths are much expensive and hard to be built in customized configurations.

Abstract

We devised a method to control the temperature of a liquid bath as low as –100oC using the duty cycle control of a solenoid valve. The solenoid valve controls the flow of liquid nitrogen that we used as a cryogen in this system. By controlling the duty cycle of a solenoid valve using feedback from the measured temperature of the liquid bath, we were able to achieve temperature stability within ±19 mK around –100oC. We also demonstrated that by taking average values of the temperature readings for sequence of measurements from more than one thermometer, it is possible to use this system for the calibration of thermometers within 3 mK. This system and the control method can be used for the precise temperature control in the range between 0oC and –100oC, where commercially available precision baths are much expensive and hard to be built in customized configurations.

참고문헌 (9)

  1. K. C. Weston, "Energy Conversion", pp.283~286 (1992), PWS Publishers
  2. W. M. Haynes, "CRC Handbook of Chemistry and Physics", pp.15~17 (2010), CRC Press
  3. H. Preston-Thomas, "The International Temperature Scale of 1990(ITS-90)", Metrologia, 27(1), pp.3~10 (1990)
  4. "IEC 60751 Ed. 2.0, Industrial platinum resistance thermometers and platinum temperature sensors", International Electrotechnical Commission, ~ (2008)
  5. W. M. Haynes, "CRC Handbook of Chemistry and Physics", pp.6~40 (2010), CRC Press
  6. 양인석, "산업용 저항 온도계의 저온 자동 비교 교정 시스템 개발", 센서학회지, 17(6), pp.429~436 (2008), 한국센서학회
  7. 양인석, "초정밀 온도센서의 저온 영역 교정 장치 개발", 센서학회지, 17(3), pp.188~194 (2008), 한국센서학회
  8. J. V. Nicholas, "Traceable Temperatures", pp.242~243 (2001), John Wiley & Sons Ltd.

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