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감마 분광분석법에 따른 방사능 국제 숙련도 시험 결과 평가

International Proficiency Test for Radioactivity by Gamma Spectroscopy Evaluation of Results

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참고문헌

키워드

주제분류방사선과학

초록

The method for verifying analytical technology in the field of radioactivity measurement involves participation in a proficiency test(PT). Proficiency tests are mandatory requirements of ISO/IEC 17025 for maintaining calibration and testing laboratories. These tests are intended to evaluate the analytical capabilities of laboratories, identify problems, support corrective actions, and verify uncertainties. We conducted a proficiency test on the Environmental Resources Association of America(ERA). In the field of radiochemistry, we participated in RAD 136 and compared our results with those of 24 lab- oratories world wide. The analytical capability of gamma nuclide was evaluated as satisfactory, warning, or unsatisfactory, according to the Z-score of ISO 13528. The radioactivity of 133Ba, 134Cs, 137Cs, 60Co and 65Zn contained in gamma emitters sample was measured and analyzed, and all the result values were satisfactory according to the Z-score evaluation criteria. Hence, we received the result Laboratory of Excellence.

Abstract

The method for verifying analytical technology in the field of radioactivity measurement involves participation in a proficiency test(PT). Proficiency tests are mandatory requirements of ISO/IEC 17025 for maintaining calibration and testing laboratories. These tests are intended to evaluate the analytical capabilities of laboratories, identify problems, support corrective actions, and verify uncertainties. We conducted a proficiency test on the Environmental Resources Association of America(ERA). In the field of radiochemistry, we participated in RAD 136 and compared our results with those of 24 lab- oratories world wide. The analytical capability of gamma nuclide was evaluated as satisfactory, warning, or unsatisfactory, according to the Z-score of ISO 13528. The radioactivity of 133Ba, 134Cs, 137Cs, 60Co and 65Zn contained in gamma emitters sample was measured and analyzed, and all the result values were satisfactory according to the Z-score evaluation criteria. Hence, we received the result Laboratory of Excellence.

참고문헌 (17)

  1. "ISO 13528:2015(E). Statistical methods for use in proficiency testing by interlaboratory comparison" (2015)[URL]
  2. "ISO/IEC 17025:2017(E). General requirements for the competence of testing and calibration laboratories" (2017)[URL]
  3. Samed OH, "Proficiency tests : A tool for improvement and testing analytical performance at Gamma-Ray Spectroscopy Laboratory", Accreditation and Quality Assurance, 22(26), pp.121~127 (2021)[DOI]
  4. Sahin NK, "A review of the nationwide proficiency test on natural radioactivity measurements by gamma spectrometry", Applied Radiation and Isotopes, 109, pp.49~53 (2016)[DOI]
  5. Dziel T, "Proficiency of 90Y and 89Sr activity measurements in Polish hospitals", Applied Radiation and Isotopes, 87, pp.24~26 (2014)[DOI]
  6. Peng EC, "A study of production of radioactive environmental reference materials used for proficiency testing program in Taiwan", Applied Radiation and Isotopes, 81, pp.14~20 (2013)[DOI]
  7. Iwahara A, "Nĺcoli IG, Alabarsa FG. Xzvier AM, et al. Proficiency test for radioactivity measurements in nuclear medicine", Journal of Radioanalytical and Nuclear Chemistry, 42(4), pp.255~259 (2009)[DOI]
  8. "Final report on the proficiency test of the Analytical Laboratories for Measurement of Environmental Radioactivity (ALMERA) network" (2005)[URL]
  9. Denis GC, "Evaluation of comparison and proficiency test results of gamma ray spectrometry at Jožef Stefan Institute from 1986 to 2014", Applied Radiation and Isotopes, 109, pp.54~60 (2016)[DOI]
  10. Halina PM, "Proficiency testing schemes on determination of radioactiviy in food and environmental samples organized by the NAEA, Poland", Nukleonika, 55(2), pp.149~154 (2010)
  11. Jin DS, "A study on the technology of measuring and analyzing neutrons and gamma-rays using a CZT semiconductor detector", Journal of Radiological Science and Technology, 45(1), pp.57~67 (2022)[DOI]
  12. Park JS, "A study on the self-absorption correction method of HPGe gamma spectrocopy analysis system using check source", Journal of Radiological Science and Technology, 45(6), pp.523~529 (2022)[DOI]
  13. "ISO 18589-3:2015(E). Measurement of radioactivity in the environment-soil- Part 3: Test method of gammaemitting radionuclides using gamma-ray spectrometry" (2015)[URL]
  14. "EML HASL-300. Method Ga-01-R: Gamma Radioassay. 4.5.2 Radiometrology" (1997)[URL]
  15. "Monographie BIPM-5"[URL]
  16. "ISO/IEC 17043:2023. Conformity assessment General requirements for the competence of proficiency testing providers" (2023)[URL]
  17. Lee JE, "Source and LVis based coincidence summing correction in HPGe gamma-ray spectrometry", Nuclear Engineering and Technology, 54(5), pp.1754~1759 (2022)[DOI]

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