Transmission Electron Microscopy Sample Preparation of Ge2Sb2Te5 Nanowire Using Electron Beam
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초록
A simple and novel transmission electron microscopy (TEM) sample preparation method for phase change nanowire is investigated. A Ge2Sb2Te5 (GST) nanowire TEM sample was meticulously prepared using nanomanipulator and gas injection system in a f eld emission scanning electron microscopy for efficient and accurate TEM analysis. The process can minimize the damage during the TEM sample preparation of the nanowires, thus enabling the crystallographic analysis of as-grown GST nanowires without unexpected phase transition caused by e-beam heating.
Abstract
A simple and novel transmission electron microscopy (TEM) sample preparation method for phase change nanowire is investigated. A Ge2Sb2Te5 (GST) nanowire TEM sample was meticulously prepared using nanomanipulator and gas injection system in a f eld emission scanning electron microscopy for efficient and accurate TEM analysis. The process can minimize the damage during the TEM sample preparation of the nanowires, thus enabling the crystallographic analysis of as-grown GST nanowires without unexpected phase transition caused by e-beam heating.
참고문헌 (12)
- Diercks D, "Techniques for consecutive TEM and atom probe tomography analysis of nanowires", Microsc. Microanal, 15(S2), pp.254~255 (2009)
- Horii H, "A novel cell technology using N-doped GeSbTe fi lms for phase change RAM", 2003 Symp. VLSI Technol, pp.177~178 (2003)
- Jung Y, "Synthesis and characterization of Ge2Sb2Te5 nanowires with memory switching effect", J. Am. Chem. Soc, 128, pp.14026~14027 (2006)
- Lee B S, "Investigation of the optical and electronic properties of Ge2Sb2Te5 phase change material in its amorphous, cubic, and hexagonal phases", J. Appl. Phys, 97, pp.093509~ (2005)
- Lee S H, "Highly scalable non-volatile and ultra-lowpower phase-change nanowire memory", Nat. Nanotechnol, 2, pp.626~630 (2007)
- Mayer J, "TEM sample preparation and FIB-induced damage", MRS Bull, 32, pp.400~407 (2007)
- Nam S W, "Electrical wind force-driven and dislocation-templated amorphization in phase-change nanowires", Science, 336, pp.1561~1566 (2012)
- Peng Y, "Nanomanipulation and electrical behaviour of a single gold nanowire using in-situ SEM-FIB-nanomanipulators", J. Phys.: Conf. Ser, 126, pp.012031~ (2008)
- Raoux S, "Phase change materials", Annu. Rev. Mater. Res, 39, pp.25~48 (2009)
- Raoux S, "Phase Change Materials: Science and Applications" (2010), Springer Science & Business Media
- Salkar R, "The sonochemical preparation of amorphous silver nanoparticles", J. Mater. Chem, 9, pp.1333~1335 (1999)
- Welnic W, "Origin of the optical contrast in phase-change materials", Phys. Rev. Lett, 98, pp.236403~ (2007)
