Cyclic microwave synthesis and characterization of cadmium tungstate particles assisted by a solid-state metathetic reaction
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Cadmium tungstate (CdWO4) particles synthesized using cyclic microwave irradiation assisted by a solid-state metathetic (SSM) reaction were well crystallized at 400-600 oC, showing a fine structure with a self-assembled rod-like morphology and a crystallographic orientation with sizes of 1-3 μm. The synthesized CdWO4 particles were characterized by X-ray diffraction,Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. The optical properties were investigated by photoluminescence emission and Raman spectroscopy.
Abstract
Cadmium tungstate (CdWO4) particles synthesized using cyclic microwave irradiation assisted by a solid-state metathetic (SSM) reaction were well crystallized at 400-600 oC, showing a fine structure with a self-assembled rod-like morphology and a crystallographic orientation with sizes of 1-3 μm. The synthesized CdWO4 particles were characterized by X-ray diffraction,Fourier transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. The optical properties were investigated by photoluminescence emission and Raman spectroscopy.
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