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Solid-state metathetic synthesis of MWO4 (M=Zn, Co) particles assisted by microwave irradiation

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초록

Metathetic route for the MWO4 (M=Zn, Co) particles is a simple method of synthesis and a viable alternative method in a short time. MWO4 (M=Zn, Co) particles were synthesized using solid-state metathetic (SSM) method with microwave irradiation. The MWO4 (M=Zn, Co) particles were formed completely at 600oC for 3 h. The crystallization process, thermal decomposition and morphology of the MWO4(M= Zn, Co) particles were evaluated. The characteristics of the SSM reaction and the formation of a high lattice energy by-product NaCl were discussed.

Abstract

Metathetic route for the MWO4 (M=Zn, Co) particles is a simple method of synthesis and a viable alternative method in a short time. MWO4 (M=Zn, Co) particles were synthesized using solid-state metathetic (SSM) method with microwave irradiation. The MWO4 (M=Zn, Co) particles were formed completely at 600oC for 3 h. The crystallization process, thermal decomposition and morphology of the MWO4(M= Zn, Co) particles were evaluated. The characteristics of the SSM reaction and the formation of a high lattice energy by-product NaCl were discussed.

참고문헌 (21)

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