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전기로 및 봉입형 응고점 셀 내의 온도구배가 미치는 표준백금저항온도계 온도측정의 불확도 요소 평가

Evaluation of Uncertainly Sources in Temperature Measurement Using Platinum Resistance Thermometer Caused by Temperature Gradient in Furnace and Sealed-type Freezing Point Cells

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참고문헌

주제분류공학일반

초록

Abstract

In the international temperature scale of 1990 (ITS-90), standard platinum resistance thermometer (SPRT) is a defining standard thermometer used in the temperature range from 13.8033 K to 961 ℃. Uncertainty of SPRT is about several mK and uncertainty of defining fixed points of the ITS-90 which is used for calibrating SPRT is about several tenth of mK. Above 0 ℃, the defining fixed points are gallium melting point and indium, tin, zinc, aluminium and silver freezing points which are all realized using an electric furnace or a liquid bath. To realize freezing point of tin (231.928 ℃) and zinc (419.527 ℃), two 3-zone furnaces which have 3 electric heaters were manufactured. Temperature gradient of the constructed furnaces were tested. Uncertainty caused by temperature gradient of furnace and immersion effect of SPRT in the sealed-type freezing point cells were evaluated 0.038 mK for tin freezing point and 0.036 mK for zinc freezing point.

참고문헌 (6)

  1. H. Preston-Thomas, "The International Temperature Scale of 1990", 27, pp.3~90 10 (1990)
  2. H. Preston-Thomas, "Supplementary Information for the International Temperature Scale of 1990", pp.35~40 (1990)
  3. T. J. Quinn, "Monographs in Physical Measurement", pp.153~164 (1990), Academic Press
  4. R. E. Bedford, "Techniques for Approximating the Internatiomal Temperature Scale of 1990"
  5. 강기훈, "핵심국제비교용 물의 삼중점 셀 제작과 비교실험 및 불확도 평가", 13(2), pp.114~120 (2004)
  6. 정명세, ""측정불확도 표현 지침(KRISS Guide to the Expression of Uncertainty in Measurement), KRISS-98-096-SP," 한국표준과학연구원, pp. 17-26, 1998.", pp.17~26 (1998), 한국표준과학연구원

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