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펄스전류활성소결법을 이용한 스퍼터링 타겟용 Cu-Mn 소결체 제조 및 특성평가

Fabrication and Property Evaluation of Cu-Mn Compacts for Sputtering Target Application by a Pulsed Current Activated Sintering Method

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주제분류금속공학

초록

Cu-Mn compacts are fabricated by the pulsed current activated sintering method (PCAS) for sputtering target application. For fabricating the compacts, optimized sintering conditions such as the temperature, pulse ratio, pressure, and heating rate are controlled during the sintering process. The final sintering temperature and heating rate required to fabricate the target materials having high density are 700oC and 80oC/min, respectively. The heating directly progresses up to 700oC with a 3 min holding time. The sputtering target materials having high relative density of 100% are fabricated by employing a uniaxial pressure of 60 MPa and a sintering temperature of 700oC without any significant change in the grain size. Also, the shrinkage displacement of the Cu-Mn target materials considerably increases with an increase in the pressure at sintering temperatures up to 700oC.

Abstract

Cu-Mn compacts are fabricated by the pulsed current activated sintering method (PCAS) for sputtering target application. For fabricating the compacts, optimized sintering conditions such as the temperature, pulse ratio, pressure, and heating rate are controlled during the sintering process. The final sintering temperature and heating rate required to fabricate the target materials having high density are 700oC and 80oC/min, respectively. The heating directly progresses up to 700oC with a 3 min holding time. The sputtering target materials having high relative density of 100% are fabricated by employing a uniaxial pressure of 60 MPa and a sintering temperature of 700oC without any significant change in the grain size. Also, the shrinkage displacement of the Cu-Mn target materials considerably increases with an increase in the pressure at sintering temperatures up to 700oC.

참고문헌 (11)

  1. G. Bertrand, , Solid-State Electron, 48, pp.505~ (2004)
  2. H. C. Kim, , J. Mater. Sci., 40, pp.2849~ (2005)
  3. H. C. Kim, , Int. J. of Refract. Met. and Hard Mater., 22, pp.197~ (2004)
  4. H. C. Kim, , Cermics Int., 34, pp.1419~ (2008)
  5. G. Bernard-Granger, , Acta Mater., 55, pp.3493~ (2007)
  6. Z. Shen, , J. Am. Ceram. Soc., 85, pp.1921~ (2002)
  7. J. E. Garay, , Appl. Phys. Lett., 85, pp.573~ (2004)
  8. J. R. Friedman, , Intermetallics, 12, pp.589~ (2004)
  9. J. E. Garay, , Acta Mater., 51, pp.4487~ (2003)
  10. H. C. Kim, , Metals and Mat. Interna, 12, pp.393~ (2006)
  11. C. Suryanarayana, "X-ray diffraction a practical approach" (1998), Plenum Press

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