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텅스텐염의 액상법을 통한 초미립 WC-Co 분말의 합성

Synthesis of Nano-sized Tungsten Carbide - Cobalt Powder by Liquid Phase Method of Tungstate

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주제분류금속공학

초록

Cemented tungsten carbide has been used in cutting tools and die materials, and is an important industrial material. When the particle size is reduced to ultrafine, the hardness and other mechanical properties are improved remarkably. Ultrafine cemented carbide with high toughness and hardness is now widely used. The objective of this study is synthesis of nanostructured WC-Co powders by liquid phase method of tungstate. The precursor powders were obtained by freezen-drying of aqueous solution of soluble salts, such as ammonium metatungstate,cobalt nitrate. the final compositions were WC-10Co. In the case of liquid phase method, it can be observed synthesis of WC-10Co. The properties of powder produced at various temperature, were estimated from the SEM, BET and C/S analyser.

Abstract

Cemented tungsten carbide has been used in cutting tools and die materials, and is an important industrial material. When the particle size is reduced to ultrafine, the hardness and other mechanical properties are improved remarkably. Ultrafine cemented carbide with high toughness and hardness is now widely used. The objective of this study is synthesis of nanostructured WC-Co powders by liquid phase method of tungstate. The precursor powders were obtained by freezen-drying of aqueous solution of soluble salts, such as ammonium metatungstate,cobalt nitrate. the final compositions were WC-10Co. In the case of liquid phase method, it can be observed synthesis of WC-10Co. The properties of powder produced at various temperature, were estimated from the SEM, BET and C/S analyser.

참고문헌 (9)

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  5. X. Xi, , Int. J. Refractory Metals & Hard Mater, 27, pp.102~ (2009)
  6. A. Voet, "Carbon Black", pp.177~ (1993), Marcel Dekker INC
  7. M. F. Zawrah, , Ceramics International, 33, pp.159~ (2007)
  8. Z. Xiong, , Int. J. Refractory Metals & Hard Mater, 26, pp.249~ (2008)
  9. S. J Park, , Int. J. Refractory Metals & Hard Mater, 26, pp.153~ (2008)

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