Formation of One-dimensional Nb2O5 Nanostructures by Anodization
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In the present work, we investigate the anodization of Nb in a K2HPO4 containing glycerol electrolyte at elevated temperatures (180oC). Under optimized conditions, uniformly over the entire anodized surface, self-organized porous Nb2O5 structures can be formed. The growth rate of highly ordered Nb2O5 is 1.7 μm/ min at beginning stage of anodization and the overall current efficiency is 70 %.
Abstract
In the present work, we investigate the anodization of Nb in a K2HPO4 containing glycerol electrolyte at elevated temperatures (180oC). Under optimized conditions, uniformly over the entire anodized surface, self-organized porous Nb2O5 structures can be formed. The growth rate of highly ordered Nb2O5 is 1.7 μm/ min at beginning stage of anodization and the overall current efficiency is 70 %.
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