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Fumed Silica 분말 소결법을 이용한 석영유리 제조에 하소 온도가 미치는 영향

The Effect of Calcination Temperature on the Synthesis of Quartz glass by Fumed Silica Sintering

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참고문헌

키워드

주제분류금속공학

초록

The quartz glasses were prepared by sintering of fumed silica powders and the effect of OH concentration on their surface on sintering was studied. Through the firing process, the fumed silica was crystallized from 1180 to 1260oC region. The amount of hydroxyl group decreased with increase in calcination temperature and consequently the crystallization was prevented. A transparent quartz glass was obtained from fumed silica, previously calcined at 1000oC,by the sintering at 1250oC for 1 h.

Abstract

The quartz glasses were prepared by sintering of fumed silica powders and the effect of OH concentration on their surface on sintering was studied. Through the firing process, the fumed silica was crystallized from 1180 to 1260oC region. The amount of hydroxyl group decreased with increase in calcination temperature and consequently the crystallization was prevented. A transparent quartz glass was obtained from fumed silica, previously calcined at 1000oC,by the sintering at 1250oC for 1 h.

참고문헌 (8)

  1. Fanderlik, "Silica Glass and its Application", pp.15~ (1991), Elsevier
  2. H. Barthel, "Organosilicon Chemistry II. From Molecules to Materials", pp.761~ (1996), VCH
  3. R. Mueller, , Powder Technol, 40, pp.140~ (2004)
  4. Y.-W. Park, , J. Korean Assoc Cryst Growth, 2, pp.47~ (1992)
  5. F. E. Wagstaff, , J. Am. Ceram Soc., 49, pp.118~ (1966)
  6. K. M. Davis, , J. Non Cryst Solids., 203, pp.27~ (1996)
  7. B. C. Bunker, , Surf. Sci., 210, pp.406~ (1989)
  8. T. Yamada, , J. Phys. Chem. C., 111, pp.12973~ (2007)

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