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가공식품 중 아크릴아마이드 분석

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참고문헌

주제분류화학

초록

Abstract

A selective analytical method of LC/MS/MS has been applied to determine the levels of acrylamidesamples includes extraction with DDDW, clean-up using C18and mixed ion exchange SPE cartridges anddetection by liquid chromatography tandem mass spectrometry. The mobile phase was a mixture of 0.1 % aceticacid and 0.5 % methanol in water. The target ions were identified and determined by ESI mass spectrometer.The overall recoveries were ranged from 91 % to 101 % and the limit of quantitation was 10 g/kg. Depending0.34 mg/kg for french fries.

참고문헌 (2)

  1. "Report of a Joint FAO", WHO Consultation (ISBN 92 2156218 8), 2002, ~
  2. "http:", ~dms, pp.acrylami.html

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