The rapid determination of PAHs in foods using ultra high performance liquid chromatography
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초록
Using a Hitachi LaChrom Ultra 2000U, a reverse phase ultra high performance liquid chromatography (u-HPLC) method was developed for the rapid quantification of 14 PAHs in foods. The proposed method for PAH analysis is based on solid phase extraction (SPE) cartridges; the determination was carried out by u-HPLC with fluorimetric detection. The method was very sensitive; PAH concentration levels were in a low μg/kg range and could be detected and quantified. Six samples of food were analyzed. Among PAHs, PHE was found in most of samples, the concentration ranging from 2.5 to 19.9 μg/kg. The contents of benzo[c]fluorine (BCL),pyrene (PYR), benzo[a]anthracene (BaA), chrysene (CHR), benzo[b]fluoranthene (BbF), benzo[k]fluoranthene (BkF) were low at the ‘μg/kg’ level or were less than LOD.
Abstract
Using a Hitachi LaChrom Ultra 2000U, a reverse phase ultra high performance liquid chromatography (u-HPLC) method was developed for the rapid quantification of 14 PAHs in foods. The proposed method for PAH analysis is based on solid phase extraction (SPE) cartridges; the determination was carried out by u-HPLC with fluorimetric detection. The method was very sensitive; PAH concentration levels were in a low μg/kg range and could be detected and quantified. Six samples of food were analyzed. Among PAHs, PHE was found in most of samples, the concentration ranging from 2.5 to 19.9 μg/kg. The contents of benzo[c]fluorine (BCL),pyrene (PYR), benzo[a]anthracene (BaA), chrysene (CHR), benzo[b]fluoranthene (BbF), benzo[k]fluoranthene (BkF) were low at the ‘μg/kg’ level or were less than LOD.
참고문헌 (21)
- S. Moret, , J. Sep. Sci, 25, pp.96~100 (2002)
- G. Purcaro, , J. Chromatogr. A, 1176, pp.231~235 (2007)
- S. Moret, , Eur. J. Lipid Sci. Technol, 107, pp.488~496 (2005)
- B. H. Chen, , J. Agric. Food Chem, 44, pp.2244~2251 (1996)
- B. H. Chen, , J. Agric. Food Chem, 45, pp.1394~1403 (1997)
- R. Weiβ Haar, , Eur. J. Lipid Sci. Technol, 104, pp.282~285 (2002)
- M. Gfrerer, , J. Sep. Sci, 26, pp.1230~1236 (2003)
- N. Kishikawa, , J. Chromatogr. B, 789, pp.257~264 (2003)
- D. Luo, , Anal. Chim. Acta, 588, pp.261~267 (2007)
- M. S. Garcia-Falcon, , J. Simal-Gandara, Food Chem, 90, pp.643~647 (2005)
- A. Stolyhwo, , Food Chem, 91, pp.303~311 (2005)
- V. H. Teixeira, , Food Chem, 104, pp.106~112 (2007)
- G. Purcaro, , J. Sep. Sci, 31, pp.3936~3944 (2008)
- M. Suchanova, , J. Sci. Food Agric, 88, pp.1307~1317 (2008)
- J. Ha, , J. AOAC Int, 93, pp.1905~1911 (2010)
- Jaeho Ha, "Rapid Method for Determination of β-Carotene in Foods Using Ultra High Performance Liquid Chromatography", Food Science and Biotechnology, 19(5), pp.1199~1204 (2010), 한국식품과학회
- M. N. Nayali-Sayadi, , Analyst, 123, pp.2145~2148 (1998)
- S. Wretling, , J. Food Compos. Anal, 23, pp.264~272 (2010)
- 허수정, "알칼리분해를 이용한 어류 중 다환방향족탄화수소의 전처리 방법", 분석과학, 18(5), pp.403~409 (2005), 한국분석과학회
- 허수정, "국내 유통 어패류 및 가공품 중 Polycyclic Aromatic Hydrocarbons 함량", 한국식품과학회지, 37(6), pp.866~872 (2005), 한국식품과학회
- 허수정, "국내유통 채소류 및 과일류 중 다환방향족탄화수소 분석", 분석과학, 19(5), pp.415~421 (2006), 한국분석과학회