섬유 보강 복합레진의 섬유 방향이 중합수축에 미치는 영향
EFFECT OF FIBER DIRECTION ON THE POLYMERIZATION SHRINKAGE OF FIBER-REINFORCED COMPOSITES
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초록
본 연구의 목적은 strain gage와 LVDT (linear variable differential transformer) 변위센서를 이용하여 섬유 보강 복합레진에서 섬유의 방향이 복합레진의 중합수축에 미치는 영향을 알아보기 위함이다. 지름 10 mm, 높이 2 mm의 원반 모양 유동성 복합레진 (Aeliteflo A2, Bisco, Inc., IL, USA) 중앙에 유리섬유 (X-80821P Glass Fiber, Bisco, Inc., IL, USA)를 위치시키고, 섬유가 배열된 장축 방향 (longitudinal)과 수직방향 (transversal)의 중합수축량을 strain gage (Linear S-series 350Ω, CAS, Seoul, Korea)를 이용하여 각각 측정하였다. 사용된 유동성 복합레진 자체의 free 중합수축을 구하기 위해 지름 7 mm, 높이 1 mm의 원반 모양 시편의 수직방향 (axial) free 중합수축값을 LVDT로 측정하였다. 중합된 시편들을 절단하여 주사전자현미경으로 복합 레진 내부 의 섬유배열을 관찰하고 각 군에서 측정된 평균 수축값들을 ANOVA로 비교하였고 Scheffe post-hoc test로 사후 검정하였다 (α=0.05). 섬유가 배열된 평면 상에서 복합레진의 중합수축 (radial shrinkage)은 섬유와 평행한 방향에서 감소하고 섬유와 수직한 방향에서 증가했다 (p<0.05). 본 연구의 결과 섬유 보강 복합레진으로 스플린트나 수복물을 제작할 때 중합수축량 은 보강된 섬유의 배열방향에 따라 큰 차이가 남을 알 수 있었다.
Abstract
The aim of this study was to evaluate the effect of fiber direction on the polymerization shrinkage of fiberreinforced composite. The disc-shaped flowable composite specimens (d = 10 mm, h = 2 mm, Aeliteflo A2, Bisco, Inc., IL, USA) with or without glass fiber bundle (X-80821P Glass Fiber, Bisco, Inc., IL, USA) inside were prepared, and the longitudinal and transversal polymerization shrinkage of the specimens on radial plane were measured with strain gages (Linear S-series 350Ω, CAS, Seoul, Korea). In order to measure the free polymerization shrinkage of the flowable composite itself, the disc-shaped specimens (d = 7mm, h = 1 mm) without fiber were prepared, and the axial shrinkage was measured with an LVDT (linear variable differential transformer) displacement sensor. The cross-section of the polymerized specimens was observed with a scanning electron microscope to examine the arrangement of the fiber bundle in composite. The mean polymerization shrinkage value of each specimen group was analyzed with ANOVA and Scheffe post-hoc test (α=0.05). The radial polymerization shrinkage of fiber-reinforced composite was decreased in the longitudinal direction of fiber, but increased in the transversal direction of fiber (p<0.05). We can conclude that the polymerization shrinkage of fiber-reinforced composite splint or restoratives is dependent on the direction of fiber.
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