Effect of Magnetic Field Annealing on Microstructure and Magnetic Properties of FeCuNbSiB Nanocrystalline Magnetic Core with High Inductance
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초록
Transverse magnetic field annealing (TFA) was carried out on Fe73.5Cu1Nb3Si15.5B7 nanocrystalline magnetic core with the aim at decreasing coercivity (Hc) while keeping high inductance (Ls). The magnetic field generated by direct current (DC) was applied on the magnetic core during different selected annealing stages and it was proved that the nanocrystalline magnetic core achieved lowest Hc when applying transverse field during the whole annealing process (TFA1). Although the microstructure and crystallization degree of the nanocrystalline magnetic core exhibited no obvious difference after TFA1 compared to no field annealing, the TFA1 sample showed a more uniform nanostructure with a smaller mean square deviation of grain size distribution. Hc of the nanocrystalline magnetic core annealed under TFA1 decreased along with the increasing magnetic field. As a result, the certain size nanocrystalline magnetic core with low Hc of 0.6 A/m, low core loss (W at 20 kHz) of 1.6 W/kg under flux density of 0.2 T and high Ls of 13.8 μH were obtained after TFA1 with the DC intensity of 140 A. The combination of high Ls with excellent magnetic properties promised this nanocrystalline alloy an outstanding economical application in high frequency transformers.
Abstract
Transverse magnetic field annealing (TFA) was carried out on Fe73.5Cu1Nb3Si15.5B7 nanocrystalline magnetic core with the aim at decreasing coercivity (Hc) while keeping high inductance (Ls). The magnetic field generated by direct current (DC) was applied on the magnetic core during different selected annealing stages and it was proved that the nanocrystalline magnetic core achieved lowest Hc when applying transverse field during the whole annealing process (TFA1). Although the microstructure and crystallization degree of the nanocrystalline magnetic core exhibited no obvious difference after TFA1 compared to no field annealing, the TFA1 sample showed a more uniform nanostructure with a smaller mean square deviation of grain size distribution. Hc of the nanocrystalline magnetic core annealed under TFA1 decreased along with the increasing magnetic field. As a result, the certain size nanocrystalline magnetic core with low Hc of 0.6 A/m, low core loss (W at 20 kHz) of 1.6 W/kg under flux density of 0.2 T and high Ls of 13.8 μH were obtained after TFA1 with the DC intensity of 140 A. The combination of high Ls with excellent magnetic properties promised this nanocrystalline alloy an outstanding economical application in high frequency transformers.
참고문헌 (23)
- Fan X D, "Soft magnetic properties in Fe84-xB10C6Cux nanocrystalline alloys", J. Magn. Magn. Mater, 326, pp.22~27 (2013)
- Flohrer S, "Random and uniform anisotropy in soft magnetic nanocrystalline alloys (invited)", J. Magn. Magn. Mater, 322, pp.1511~1514 (2010)
- Fujii H, "Nanocrystallization of Fe73.5Si13.5B9Nb3Cu1 soft-magnetic alloy from amorphous precursor in a magnetic field", J. Mater. Sci, 43, pp.3837~3847 (2008)
- Herzer G, "Grain size dependence of coercivity and permeability in nanocrystalline ferromagnets", IEEE Trans. Magn, 26, pp.1397~1402 (1990)
- Herzer G, "Nanocrystalline soft magnetic materials", J. Magn. Magn. Mater, 112, pp.258~262 (1992)
- Herzer G, "Soft magnetic nanocrystalline materials", Scripta Metall. Mater, 33, pp.1741~1756 (1995)
- Herzer G, "Handbook of Magnetic Materials", pp.415~462 (1997), Elsevier Science Pub
- Herzer G, "Anisotropies in soft magnetic nanocrystalline alloys", J. Magn. Magn. Mater, 294, pp.99~106 (2005)
- Herzer G, "Modern soft magnets: amorphous and nanocrystalline materials", Acta. Mater, 67, pp.718~734 (2013)
- Hono K, "Cu clustering and Si partitioning in the early crystallization stage of an Fe73.5Si13.5B9Nb3Cu1amorphous alloy", Acta Mater, 47, pp.997~1006 (1999)
- Ito N, "Effect of magnetic field annealing on the soft magnetic properties of nanocrystalline materials", J. Magn. Magn. Mater, 316, pp.458~461 (2007)
- Makino A, "Nanocrystalline soft magnetic Fe-Si-B-P-Cu alloys with high B of 1.8-1.9T contributable to energy saving", IEEE Trans. Magn, 48, pp.1331~1335 (2012)
- Makino A, "Nanocrystalline soft magnetic Fe-M-B (M=Zr, Hf, Nb) alloys produced by crystallization of amorphous phase (overview)", Mater. Trans. JIM, 36, pp.924~938 (1995)
- Miglierini M, "In situ crystallization of metallic glasses during magnetic field annealing", Acta Mater, 91, pp.50~56 (2015)
- Ohta M, "Magnetic properties of nanocrystalline Fe82.65Cu1.35SixB16-x alloys (x=0-7)", Appl. Phys. Lett, 91, pp.062517~ (2007)
- Ohta M, "Magnetic properties of high-Bs Fe-Cu-Si-B nanocrystalline soft magnetic alloys", J. Magn. Magn. Mater, 320, pp.e750~e753 (2008)
- Onodera R, "Nucleation control for fine nano crystallization of Fe-based amorphous alloy by high-magnetic-field annealing", J. Alloy. Compd, 637, pp.213~218 (2015)
- Suzuki K, "Magnetic-field-induced anisotropies and exchange softening in Fe-rich nanocrystalline soft magnetic alloys", Scripta Mater, 67, pp.548~553 (2012)
- Suzuki K, "Soft magnetic properties of nanocrystalline bcc Fe-Zr-B and Fe-M-B-Cu (M=transition metal) alloys with high saturation magnetization (invited)", J. Appl. Phys, 70, pp.6232~6237 (1991)
- Suzuki K, "High saturation magnetization and soft magnetic properties of bcc Fe-Zr-B and Fe-Zr-B-M (M=transition metal) alloys with nanoscale grain size", Mater. Trans. JIM, 32, pp.93~102 (1991)
- Willard M A, "Structure and magnetic properties of (Fe0.5Co0.5)88Zr7B4Cu1 nanocrystalline alloys", J. Appl. Phys, 84, pp.6773~6777 (1998)
- Yoshizawa Y, "New Fe-based soft magnetic alloys composed of ultrafine grain structure", J. Appl. Phys, 64, pp.6044~6046 (1988)
- Yoshizawa Y, "Fe-based soft magnetic alloys composed of ultrafine grain structure", Mater Trans. JIM, 31, pp.307~314 (1990)
