Green synthesis and characterization of Ni /NiO magnetic nanoparticles in water
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Ni/NiO magnetic nanoparticles was prepared using Ni(CH3COO)2 4H2O as starting material, acetylacetonate (AcAc) as template and water as a green solvent under reflux condition, followed by the calcination at 400 o C. The product was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Fourier transform infrared (FT-IR). The size distribution of individual particles were determined to be about 18-20 nm. The prepared magnetic nanoparticles was found to be a good adsorbent for Congo red from solution.
Abstract
Ni/NiO magnetic nanoparticles was prepared using Ni(CH3COO)2 4H2O as starting material, acetylacetonate (AcAc) as template and water as a green solvent under reflux condition, followed by the calcination at 400 o C. The product was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Fourier transform infrared (FT-IR). The size distribution of individual particles were determined to be about 18-20 nm. The prepared magnetic nanoparticles was found to be a good adsorbent for Congo red from solution.
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