액중 전기선폭발법으로 제조된 구리 나노콜로이드의 특성 평가
Evaluation of Cu nano-colloid prepared by electrical wire explosion in liquid phase
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초록
Cu nano-colloid was prepared by wire electric explosion process under de-mineralized water and anhydrous ethanol. To control the properties of Cu nano-colloid, experimental conditions such as diameter of Cu wire and applied voltage were changed. The optimal Cu nano-colloid was prepared when the 0.1㎜ diameter of Cu wire with the applied voltage of 2000 V was used. The shape of Cu particles in colloid was spherical and the XRD result revealed that the phase of Cu particles was cubic phase. About 20㎚ Cu nanoparticles with high crystallinity were successfully prepared using wire explosion process under anhydrous ethanol and they showed more than 100 hours dispersion stability.
Abstract
Cu nano-colloid was prepared by wire electric explosion process under de-mineralized water and anhydrous ethanol. To control the properties of Cu nano-colloid, experimental conditions such as diameter of Cu wire and applied voltage were changed. The optimal Cu nano-colloid was prepared when the 0.1㎜ diameter of Cu wire with the applied voltage of 2000 V was used. The shape of Cu particles in colloid was spherical and the XRD result revealed that the phase of Cu particles was cubic phase. About 20㎚ Cu nanoparticles with high crystallinity were successfully prepared using wire explosion process under anhydrous ethanol and they showed more than 100 hours dispersion stability.
참고문헌 (32)
- Abraham, T, "Nanostructured materials : An overview and commercial analysis", Journal of Metals, 50(1), pp.36~37 (1998)
- Kim, B. K., , Journal of Korean Powder Metallurgy Institute, 9, pp.324~ (2002)
- Gary, A., "Science and Technology of nanostructured magnetic materials", pp.1~176 (1991), Plenum press
- Kim, Y. H., "The effect of zeta-potential on the stabilization of silver nanoparticle colloid prepared by alcohol reduction method with PVP", Journal of Korean Industrial and Engineering Chemistry, 14(4), pp.487~492 (2003)
- Back, I. H., "Stabilization of nanometer-sized sil ver-ethylene glycol colloid prepared with using ployacrylamide-co-acrylic acid", Journal of Korean Industrial and Engineering Chemistry, 15, pp.402~406 (2004)
- Back, I. H., "Stabilization of nanometer-sized sil ver-ethylene glycol colloid prepared with using ployacrylamide-co-acrylic acid", Journal of Korean Industrial and Engineering Chemistry, 15, pp.402~406 (2004)
- Gleiter, H., "Nanostructured materials : Basic concepts and microstructure", Acta materialia, 48, pp.1~29 (2000)
- Cahill, David, G., "Nanofluids for thermal transport", Materials Today, 8, pp.36~44 (2005)
- Chace, W. G, "Exploding wires" (1964), Plenum press
- Agnew, S. R., "Microstructure and mechanical behavior of nanocrystalline metal", Materials Science and Engineering, 285(1-2), pp.391~396 (2000)
- Kotov, Y. A., "Production of nanometer sized A1N powder by the explosion wire method", Nanostructured Materials, 12, pp.119~122 (1999)
- Chung, K. S., "Synthesis of highly concentrated TiO2 nanocolloids and coating on boron nitride powder", Colloids and Surfaces A, pp.175~178 (2008)
- Kim, J. H., "Preparation of copper foam with 3-dimensionally interconnected spherical pore network by electrodeposition", Electrochemistry Communications, 10, pp.1148~1151 (2008)
- Huang, L., "Electrodeposition of monodisperse copper nanoparticles on highly oriented pyrolytic graphite electrode with modulation potential method", Colloids and Surfaces A, 262, pp.125~131 (2005)
- Huang, L., "Electrodeposition of monodisperse copper nanoparticles on highly oriented pyrolytic graphite electrode with modulation potential method", Colloids and Surfaces A, 262, pp.125~131 (2005)
- Furumi, S., "Micro-emulsion synthesis of blue-luminescent silicon nanoparticles stabilized with alkoxy monolayers", Journal of Crystal Growth, 311, pp.643~637 (2009)
- Meng, S., "Preparation of micron size copper powder with chemical reduction method", materials letters, 60, pp.2438~2442 (2006)
- Im, S., "Preparation of ultrafine nanoparticles in surfactant aggregate as a reaction medium", Applied Chemistry, 3, pp.168~ (1999)
- Chang, W., "Chemical vapor condensation of nanostructured ceramic powders", Nanostructured Materials, 4(3), pp.345~351 (1994)
- Guk, Y. H., "Colloid and Surfactant", pp.86~114 (1995), Dae Kwang
- Jiang, W., "Pulsed wire Discharge for nanosized Powedr Synthesis", Institute of Electrical and Electronics Engineers Transaction on Plasma Science, 26(5), pp.1498~1501 (1998)
- Shi, J., "One-step synthesis of the nanometer particles of ɤ-Fe2O3 by wire electrical explosion method", Materials Research Bulletin, 36, pp.503~509 (2001)
- Kim, J. S., "Ultra-fine powder by wire explosion method", Scripta materialia, 44, pp.2247~2251 (2001)
- Beketov, T. I., "Characteristics of ZrO2 nanopowders produced by electrical explosion of wire", Journal of Aerosol Science, 26, pp.905~906 (1995)
- Chakravarthy, S. R., "Understanding nanoparticle formation by a wire explosion process through experimental and modelling studies", Nanotechnology, 19, pp.1~11 (2008)
- Guangtian Z., "Thermal characteristic of ultrafine-grained aluminum produced by wire electrical explosion", Scripta materialia, 44, pp.17~23 (2001)
- De Groot, J. S., "Homogeneous electrical explosion of tungsten wire in vaccum", Journal of Experimental and Theoretical Physics Letter, 73, pp.69~74 (2001)
- Kortkhonjia, V. P., "On the role of exothermal chemical reaction during wire explosion in water", Techenical Physics Letter, 29, pp.797~800 (2003)
- Gerhard, E., "The fundamentals of nano-and submicro-scaled ceramic particles incorporation into electrodeposited nickel layers : Zeta potential measurements", Surface & Coating Technology, 203, pp.1806~1814 (2009)
- Li, X., "Evaluation on dispersion behavior of the aqueous copper nanosuspensions", Journal of colloid and Interface Science, 310, pp.456~463 (2007)
- Ahn, Y. C., "Production and dispersion stability of nanoparticles in nanofluids", Powder Technology, 186, pp.145~153 (2008)
- Jung, S. J., "Effect of the concentration of suspension and electrolyte on zeta potential", Journal of the Korean ceramic Society, 40, pp.293~300 (2003)
