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전자코 시스템을 이용한 우유의 품질에 따른 휘발성 향기성분 분석

Analysis of Volatile Flavor Compounds in Milk Using Electronic Nose System

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초록

Volatile flavor compounds from milk were analyzed and identified by using the analysis methods of headspace solid phase microextraction gas chromatography/mass spectrometry (HSPME-GC/MS) and electronic nose (E-Nose) system. About 30 volatile compounds were identified by HSPME-GC/MS for the fresh and off-flavor milk samples. Also, the correlation between rancidity and ageing days of milk was obtained by the aid of principal component analysis algorithm. It shows that the E-Nose system can identify the various types of milk flavor. These results imply that the analysis method based on the E-nose system can apply to the quality control of milk flavor and the rancidity.

Abstract

Volatile flavor compounds from milk were analyzed and identified by using the analysis methods of headspace solid phase microextraction gas chromatography/mass spectrometry (HSPME-GC/MS) and electronic nose (E-Nose) system. About 30 volatile compounds were identified by HSPME-GC/MS for the fresh and off-flavor milk samples. Also, the correlation between rancidity and ageing days of milk was obtained by the aid of principal component analysis algorithm. It shows that the E-Nose system can identify the various types of milk flavor. These results imply that the analysis method based on the E-nose system can apply to the quality control of milk flavor and the rancidity.

참고문헌 (10)

  1. E. Valero, "Changes in flavour and volatile components during storage of whole and skimmed UHT milk", Food Chem., 72(1), pp.51~58 (2001)
  2. B. Toso, "Determination of volatile compounds in cows’ milk using headspace GCMS", J. Dairy Res., 69, pp.569~577 (2002)
  3. M. M. Calvo, "Flavour of heated milks. A review", Int. Dairy J., 2(2), pp.69~81 (1992)
  4. K. R. Christensen, "Gas chromatographic analysis of volatile sulfur compounds from heated milk using static headspace sampling", J. Dairy Sci., 75, pp.2098~2104 (1992)
  5. B. Wang, "Application of the electronic nose to the identification of different milk flavorings", Food Res. Int., 43(1), pp.255~262 (2010)
  6. A. Loutfi, "Electronic noses for food quality: A review", J. Food Eng., 144, pp.103~111 (2015)
  7. M. P. Villeneuve, "Milk volatile organic compounds and fatty acid profile in cows fed timothy as hay, pasture, or silage", J. dairy Sci., 96(11), pp.7181~7194 (2013)
  8. R. R. Early, "Effect of process and temperature during storage on ultra-high temperature steaminjected milk", J. Dairy Sci., 65(1), pp.11~16 (1982)
  9. I. J. Jeon, "Production of volatile flavor compounds in ultrahigh-temperature processed milk during aseptic storage", J. Agric. Food Chem., 26(5), pp.1183~1188 (1978)
  10. B. E. Loney, "Chemical and flavor changes in sterile concentrated milk during storage", J. Dairy Sci., 51(11), pp.1770~1775 (1968)

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