천연인디고를 이용한 셀룰로오스계 직물 염색의 표준화 연구: 일단계 환원/염색에 의한 마직물 염색
Optimization of Cellulose Dyeing with Natural Indigo: Ramie dyeing by One-step Reduction/dyeing Process
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One-step reduction/dyeing method was applied for ramie dyeing with natural indigo powder. The effect of reduction/dyeing conditions including the pH of bath, dye temperature and time, and concentration of indigo powder and reduction agent on dye uptake and color properties were investigated. Regardless of addition of alkali, the dyed fabrics appeared in the PB Munsell color range(λmax: 660 nm) and the dye uptake was much higher with no addition of sodium hydroxide. Dyeing was carried out through the use of only sodium hydrosulfite in the bath. The maximum dye uptake was obtained at 60 for 30min. Saturated dye uptake was obtained at 2 g/L of sodium hydrosulfite concentration up to 2 g/L of indigo powder. Whereas, at higher indigo powder concentration (4 g/L), more than 3 g/L of reducing agent concentration was required for obtaining the saturated dye uptake. Color reproducibility was reliable with color difference in the range of 0.03~0.16. Regardless of color strength, fastness to rubbing was acceptable with a 3/4~4/5. Fastness to washing, dry cleaning, and light of samples with low color strength were poor. Whereas, fastness to washing, dry cleaning,and light of samples with high color strength were very good.
Abstract
One-step reduction/dyeing method was applied for ramie dyeing with natural indigo powder. The effect of reduction/dyeing conditions including the pH of bath, dye temperature and time, and concentration of indigo powder and reduction agent on dye uptake and color properties were investigated. Regardless of addition of alkali, the dyed fabrics appeared in the PB Munsell color range(λmax: 660 nm) and the dye uptake was much higher with no addition of sodium hydroxide. Dyeing was carried out through the use of only sodium hydrosulfite in the bath. The maximum dye uptake was obtained at 60 for 30min. Saturated dye uptake was obtained at 2 g/L of sodium hydrosulfite concentration up to 2 g/L of indigo powder. Whereas, at higher indigo powder concentration (4 g/L), more than 3 g/L of reducing agent concentration was required for obtaining the saturated dye uptake. Color reproducibility was reliable with color difference in the range of 0.03~0.16. Regardless of color strength, fastness to rubbing was acceptable with a 3/4~4/5. Fastness to washing, dry cleaning, and light of samples with low color strength were poor. Whereas, fastness to washing, dry cleaning,and light of samples with high color strength were very good.
참고문헌 (23)
- 강지연, "천연 쪽을 이용한 양모 섬유의 염색 (I)", 한국염색가공학회지, 13(4), pp.15~22 (2001)
- 김미경, "쪽을 이용한 천연염색 시 조건에 따른 면직질의 염 색성에 관한 연구", 석사, pp.2010
- 김상률, "천연물질을 활용한 웰빙기법 천연염색에 관한 연구 (2) -소엽염색 면직물의 모나자이트 처리효과-", 한국의류산업학회지, 12(2), pp.240~245 (2010), 한국의류산업학회
- 김성련, "피복재료학", pp.69~71 (2000), 교문사
- 손경희, "일단계 환원", 염색에 의한 모직물의 천연인디고 염색, 2010, pp.34(3), 508~517[DOI]
- 송성원, "쪽 염료의 제조와 염색법에 관한 연구", 석사, pp.2008
- 송성원, "건조 쪽잎 추출액에 의한 면직물 염색성", 한국염색가공학회지, 20(3), pp.18~24 (2008), 한국염색가공학회
- 신윤숙, "Tencel Dyeing by Natural Indigo Prepared from Dyer's Knotweed", 한국의류학회지, 32(12), pp.1963~1970 (2008), 한국의류학회
- 신윤숙, "생쪽잎분말의 염색성 및 저장성 (Ⅰ) - 동결건조방법 -", 한국염색가공학회지, 21(1), pp.10~20 (2009), 한국염색가공학회
- 신윤숙, "생쪽잎분말의 염색성 및 저장성(Ⅱ) - 열풍 및 상온건조방법 -", 한국염색가공학회지, 21(4), pp.23~32 (2009), 한국염색가공학회
- 신윤숙, "포도당 환원을 이용한 천연 인디고 염색", 한국염색가공학회지, 21(3), pp.10~18 (2009), 한국염색가공학회
- 신윤숙, "면직물에의 천연 인디고 염색 - 일단계 환원", 염색 공정 -, 2010, pp.22(2), 101~109[DOI]
- 유명님, "델파이법을 이용한 천연염색에 관한 기초 연구 (제3보)-천연염료의 개발가치 평가-", 한국의류학회지, 30(5), pp.733~741 (2006), 한국의류학회
- 이종남, "우리가 정말 알아야 할 천연염색", pp.278~293 (2004), (주)현암사
- 정인모, "쪽 색소에 의한 견섬유 염색에 관한 연구: 발효염색에 대하여", 한국잠사학회지, 40(1), pp.78~85 (1998)
- 조경래, "규합총서에 나타난 전통염색법해설", pp.123~128 (2007), 한국학술 정보(주)
- 홍병숙, "친환경 유·아동 속옷 소비자의 환경친화적 태도와 의복추구혜택이 구매만족도에 미치는 영향", 한국의류학회지, 34(4), pp.686~696 (2010), 한국의류학회
- 황은경, "Vat 염료에 의한 견섬유의 염색에 관한 연구", 한국잠사학회지, 38(2), pp.198~174 (1996)
- Bechtold, T, "Natural dyes for textile dyeing: A comparison of methods to assess the quality of Canadian golden rod plant material", Dyes and Pigments, 75, pp.287~293 (2007)
- Blackburn, R. S, "The development of indigo reduction methods and pre-reduced indigo products", Coloration Technology, 125, pp.193~207 (2009)
- Etters, J. N, "Equilibrium sorption isotherms of indigo on cotton denim yarn: Effect of pH", Textile Research Journal, 61(12), pp.773~776 (1991)
- Kunttou, K, "Dyeing polyester fabrics with indigo", Textiles Research Journal, 75(2), pp.149~153 (2005)
- Weissbein, L, "The physical state of direct dyes in viscose and its influence on lightfastness", Textiles Research Journal, 30(1), pp.58~62 (1960)