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실용화를 위한 쪽 염료의 관한 연구

Study on the Development of Practical Application of Indigo Dyes

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주제분류생활과학

초록

The process of making or cultivating indigo dyes is very cumbersome and complex. The dye extraction and dyeing methods using general plant dye, moth repellent dye, fast acting natural dye, and other dyes are very different. This research investigates the extraction of indigo dye and liquid dye extraction of polygonum(indigo) plants using calcium oxide water. While extracting indigo dye the concentration of purified indigo dye may be controlled by adjusting the pH level. Due to the various uses of dyes the adjustment of surface color must be considered. In regard to the change according to different concentrations of reducing agents, it was found that cotton fabrics and ramie fabrics show the highest color difference at 0.4% and 0.3% respectively. As the reduction temperature increases, the color difference increases as well. The maximum color difference was found to appear at 90℃. Cotton fabrics and ramie fabrics showed 70.55 and 67.01 respectively. The color difference increases as the concentration of dyes increases, but at a concentration of 300%, cotton fabrics was found to show 6.22PB in H value using the Munsell color system, containing purple and blue color. The pH of the polygonum dyes extracted through this experiment were adjusted by adding calcium oxide to the experimental water, without directly adding calcium oxide to the liquid polygonum extract. In a refine state, it was mixed with polygonum extract to extract a more refine and highly concentrated indigo dye. When lye and reducing agents are added to extracted indigo dye and sealed for long-term storage, it can be effective and easily used for dyeing.

Abstract

The process of making or cultivating indigo dyes is very cumbersome and complex. The dye extraction and dyeing methods using general plant dye, moth repellent dye, fast acting natural dye, and other dyes are very different. This research investigates the extraction of indigo dye and liquid dye extraction of polygonum(indigo) plants using calcium oxide water. While extracting indigo dye the concentration of purified indigo dye may be controlled by adjusting the pH level. Due to the various uses of dyes the adjustment of surface color must be considered. In regard to the change according to different concentrations of reducing agents, it was found that cotton fabrics and ramie fabrics show the highest color difference at 0.4% and 0.3% respectively. As the reduction temperature increases, the color difference increases as well. The maximum color difference was found to appear at 90℃. Cotton fabrics and ramie fabrics showed 70.55 and 67.01 respectively. The color difference increases as the concentration of dyes increases, but at a concentration of 300%, cotton fabrics was found to show 6.22PB in H value using the Munsell color system, containing purple and blue color. The pH of the polygonum dyes extracted through this experiment were adjusted by adding calcium oxide to the experimental water, without directly adding calcium oxide to the liquid polygonum extract. In a refine state, it was mixed with polygonum extract to extract a more refine and highly concentrated indigo dye. When lye and reducing agents are added to extracted indigo dye and sealed for long-term storage, it can be effective and easily used for dyeing.

참고문헌 (15)

  1. 강지연, "천연 쪽을 이용한 양모 섬유의 염색(Ⅰ)", 한국염색가공학회지, 13(4) (2001)
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  9. 임용진, "건조 쪽으로부터 인디고의 추출 방법", 특허출원, ~ (2001)
  10. 정인모, "쪽색소에 의한 絹織維염색에 관한 연구", 한국잠사학회지, 40(1) (1998)
  11. 정인모, "환원제 Sodium Hydrosulfite를 이용한 천연 쪽의 견 염색 효과", 한국잠사학회지, 44(2) (2002)
  12. 정인모, "명주의 전통 쪽 염색 방법에 관한 연구", 한국잠사학회지, 47(1) (2005)
  13. 정인모, "천연 인디고 색소의 구조분석", 한국잠사학회지, 49(1) (2007)
  14. 조영미, "전통 남염색에 관한 연구", 석사, pp.1995
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