본문 바로가기
KERD
논문KCI 등재

환경숙련도 시험에서의 평가기준 설정

Evaluation Criteria for Proficiency Testing in Environmental Samples of Water, Drinking Water, Waste and Soil Field

0

조회

0

다운로드

2

인용

0

참고문헌

키워드

초록

This study was performed in order to establish a reasonable assigned value and target standard deviation invarious matrices from proficiency test results. RPDs between manufactured PT sample concentrations androbust or normal averages were lower than 5% in almost all items except in water, drinking water, waste andsoil and 5% to 9.5% in organic solvents and organo-phosphate pesticides. Robust averages and robust standarddeviations from 2002 to 2012 were calculated and Coefficient of variation (CV) was used as statistical toolsto find the target standard deviation in each fields. As a result, CV of all items except mercury and arsenicshowed less than 10% in water and drinking water fields. CV of mercury and arsenic was less than 20%. Mostitems of heavy metal in waste and soil showed less than 15%. Therefore, it is determined to be reasonable thatthe standard deviation of future itemized goal is calculated by multiplying the coefficient of variation of thestatistical processing results during 11 years. These results will contribute to providing reliable evaluation criteriaand relevant information when establishing the PT evaluation guidelines according to ISO 17043 in various fields.

Abstract

This study was performed in order to establish a reasonable assigned value and target standard deviation invarious matrices from proficiency test results. RPDs between manufactured PT sample concentrations androbust or normal averages were lower than 5% in almost all items except in water, drinking water, waste andsoil and 5% to 9.5% in organic solvents and organo-phosphate pesticides. Robust averages and robust standarddeviations from 2002 to 2012 were calculated and Coefficient of variation (CV) was used as statistical toolsto find the target standard deviation in each fields. As a result, CV of all items except mercury and arsenicshowed less than 10% in water and drinking water fields. CV of mercury and arsenic was less than 20%. Mostitems of heavy metal in waste and soil showed less than 15%. Therefore, it is determined to be reasonable thatthe standard deviation of future itemized goal is calculated by multiplying the coefficient of variation of thestatistical processing results during 11 years. These results will contribute to providing reliable evaluation criteriaand relevant information when establishing the PT evaluation guidelines according to ISO 17043 in variousfields.

참고문헌 (19)

  1. 김우일, "폐절연유를 이용한 숙련도 평가용 PCBs 표준물질의 적용성 평가", 분석과학, 23(3), pp.247~254 (2010), 한국분석과학회
  2. 박경환, "숙련도시험을 통한 시험환경 신뢰성 향상에 관한 연구", 석사, 벤처전문기술학, pp.2009
  3. "ISO", IEC 17025, General requirements for the competence of testing and calibration laboratories, 2005, pp.1~28
  4. "ISO", IEC 17043, Conformity assessment-General requirements for proficiency testing, 2012, pp.1~39
  5. "ISO", IEC 13528, Statistical methods for use in proficiency testing by interlaboratory comparisons, 2002, pp.1~66
  6. 장희라, "농약 이화학시험 분석기관의 숙련도시험을 통한 정도관리체계 확립 연구", 농약과학회지, 16(4), pp.350~356 (2012), 한국농약과학회
  7. Qi Zhou, "Use of robust zB and zW to evaluate proficiency testing data", Clinica Chimica Acta, 412, pp.936~939 (2011)
  8. Qi Zhou, "Detection of outliers and establishment of targets in external quality assessment programs", Clinica Chimica Acta, 372, pp.94~97 (2006)
  9. "Proficiency testing Australia" (2014)[URL]
  10. 이낙영, "숙련도시험자료에 대한 통계적 분석방법", 충남과학연구지, 28(1), pp.12~18 (2001)
  11. "IFA" (2013)[URL]
  12. Kenneth J. Caviston, "National Air Toxics Trends Stations (NATTS) Proficiency Testing Program", pp.1~26 (2005), U.S. Environmental Protection Agency Office of Air Quality Planning and standards Research triangle Park Publishing
  13. "ISO Guide 35, Certification of reference materials-General and statistical principles", 1~64 (2006)
  14. Environmental Resource Associates (ERA), "Performance report of water pollution", 1~18 (2011)
  15. Environmental Resource Associates (ERA), "Performance report of water pollution", 1~10 (2012)
  16. Environmental Resource Associates(ERA), "Performance report of water supply", 1~14 (2011)
  17. Environmental Resource Associates(ERA), "Performance report of water supply", 1~13 (2012)
  18. M. Thompson, "The international harmonized protocol for the proficiency testing of analytical chemistry laboratories (IUPAC Technical Report)", Pure Appl. Chem, 78(1), pp.145~197 (2006)
  19. Environmental Resource Associates(ERA), "Performance report of soils & hazardous waste", 1~13 (2011)

관련 논문AI추천

토양 숙련도 시험용 금속 표준시료(PTMs) 제조방법 확립 및 적용성 평가김지영, 이석기, 이원석, 이진선, 홍석영한국환경분석학회 · 환경분석과 독성보건2016 · 제19권 제2호수질 중 중금속(Cr, Ba) 숙련도 시험 평가김윤석, 서대근, 송대성, 이정엽, 이종운, 최재원한국환경분석학회 · 환경분석과 독성보건2018 · 제21권 제1호중금속분석용 하천수 매질표준물질을 이용한 숙련도 결과 평가강학구, 김영희, 김일규, 김현정, 송기봉, 신선경, 안희주, 이수영한국분석과학회 · 분석과학2010 · 제23권 제3호환경분야 시험 · 검사기관의 정도관리 현장평가결과 고찰고상호, 김명진, 김지혜, 박현우, 이경로, 이수영, 이진주, 이혜리, 전수아, 정현미, 최성헌, 최종우, 허유정, 홍석영, 황종연한국환경분석학회 · 환경분석과 독성보건2019 · 제22권 제4호수질 중 유기인계 농약류, Diazinon과Parathion의 숙련도 시험용 시료 개발김윤석, 이정엽, 정영철, 최원석, 최재원한국환경분석학회 · 환경분석과 독성보건2017 · 제20권 제2호환경분야 시험 · 검사방법의 유효성 검증 기법 연구고상호, 김금희, 김명옥, 김명진, 김지혜, 유은진, 윤숙희, 이신우, 이진주, 임보라, 정현미, 최종우, 허유정, 홍석영, 황종연한국환경분석학회 · 환경분석과 독성보건2018 · 제21권 제2호

이 간행물의 다른 논문 (6건)