논문KCI 등재
A Simple, Efficient, Catalyst-Free and Solvent-Less Microwave-Assisted Process for N-Cbz Protection of Several Amines
2
조회
0
다운로드
0
인용
0
참고문헌
키워드
주제분류화학
초록
A simple, green and chemo-selective method for the N-benzyloxycarbonylation of amines, β-amino alcohols, α- amino esters and sulfonamides has been developed under microwave irradiation. Good to excellent yields of the N-benzyloxycarbamates compounds were obtained in short times without any side products.
Abstract
A simple, green and chemo-selective method for the N-benzyloxycarbonylation of amines, β-amino alcohols, α- amino esters and sulfonamides has been developed under microwave irradiation. Good to excellent yields of the N-benzyloxycarbamates compounds were obtained in short times without any side products.
참고문헌 (25)
- Greene, T. W., "Greene's Protective Groups in Organic Synthesis" (2007), Wiley
- Kocienski, P. J., "Protecting Groups" (2004), George Thieme Verlage
- TaekHyeonKim, "N-Benzyloxycarbonyl-2-methylaminothiazoline as a SelectiveBenzyloxycarbonylating Reagent of Amines", Bulletin of the Korean Chemical Society, 24(2), pp.157~158 (2003), 대한화학회
- Sajiki, H., , Tetrahedron Lett, 36, pp.3465~ (1995)
- Kumar, V. P., , Tetrahedron Lett, 47, pp.6393~ (2006)
- Hernandez, J. N., , J. Org. Chem, 69, pp.3590~ (2004)
- Babu, K. S, , Can. J. Chem, 87, pp.393~ (2009)
- Gawante, M. B., , Tetrahedron Lett, 48, pp.8170~ (2006)
- Mahesh, K. C, , Tetrahedron Lett, 48, pp.55~ (2007)
- Varala, R, , J. Iran. Chem. Soc, 4, pp.370~ (2007)
- Suryakiran, N., , Tetrahedron Lett, 49, pp.2607~ (2008)
- Shkhande, J., , Tetrahedron Lett, 49, pp.4799~ (2008)
- Zhang, C. L, , Chem. Lett, 23, pp.789~ (2012)
- Yadav, V. K, , J. Org. Chem, 69, pp.577~ (2004)
- Bora, P. P, , Synth. Commu, 41, pp.2674~ (2011)
- Larhed, M, "Micowave Methods in Organic Synthesis" (2006), Sringger-Verlag
- Gedye, R, , Tetrahedron Lett, 27, pp.279~ (1986)
- Guiguere, R. J., , Tetrahedron Lett, 27, pp.4954~ (1986)
- K’tir, H, , Chem. Lett, 43, pp.851~ (2014)
- Lakrout, S, , RSC. Adv, 4, pp.16027~ (2014)
- Ouarna, S, , J. Orient. Chem, 31, pp.2~ (2015)
- Mansouri, R., , J. Braz. Chem. Soc, 3, pp.546~ (2016)
- Amira, A., "Synthèse, Réactivité et Evaluation de l’Activité Biologique d’Hétérocycles Azotés : Conception de Nouveaux Agents Alkylants & Protection N-Boc d’Amines Assistée par Ultrasons", Ph. D., pp.2015
- Amira, A, , Der. Pharma. Chemica, 7, pp.213~ (2015)
- Höck, S, , CHIMIA, 64, pp.200~ (2010)
이 간행물의 다른 논문 (13건)
Photoacoustic Effect of Ethene: Sound Generation due to Plant Hormone Gases박한정, David W. Idepp. 139-142역류산화공정을 이용한 고농도 PCBs 함유 절연유의 처리유건상, 김대익, 이창순pp. 143-150One Pot Four-Component Synthesis of Novel Substituted 2-Phenyl-4(3H) Quinazolinones Using Recyclable Nanocrystalline CuMnO3 CatalystG. B. Dabhade, A. V. Borhade, D. R. Tope, G. D. Garepp. 157-162Mn4+ 도핑된 형광체, Sr1−xBaxGe4O9:Mn4+0.005 (0.00 ≤ x ≤ 1.00)의 Color Tuning박운배pp. 163-167Enhanced Photocatalytic Properties of Visible Light Responsive La/TiO2-Graphene Composites for the Removal of Rhodamin B in Water오원춘, Yonrapach Areerobpp. 168-178