본문 바로가기
KERD
논문

SiC 세라믹스의 균열치유거동 및 부식특성

Crack-healing Behavior and Corrosion Characteristics of SiC Ceramics

0

조회

0

다운로드

2

인용

0

참고문헌

키워드

주제분류해양공학

초록

The crack‐healing behavior and corrosion resistance of SiC ceramics were investigated. Heat treatments were carried out from 900 ℃to 1300 ℃. A corrosion test of SiC was carried out in acid and alkaline solutions under KSL1607. The results showed that heat treatment in air could significantly increase the strength. The heat‐treatment temperature has a profound influence on the extent of crack healing and the degree of strength recovery. The optimum heat‐treatment temperature was 1100 ℃ for one hour at an atmospheric level. In the two kinds of solutions, the cracks in a specimen were reduced with increasing time, and the surface of the crack healed specimen had a greater number of black and white spots. The strength of the corroded cracked specimen was similar to that of the cracked specimen. The strength of the corroded crack healed specimen decreased 47% and 75% compared to that of the crack healed specimen in the acid and alkaline solutions, respectively. Therefore, the corrosion of SiC ceramics is faster in an alkaline solution than in an acid solution.

Abstract

The crack‐healing behavior and corrosion resistance of SiC ceramics were investigated. Heat treatments were carried out from 900 ℃to 1300 ℃. A corrosion test of SiC was carried out in acid and alkaline solutions under KSL1607. The results showed that heat treatment in air could significantly increase the strength. The heat‐treatment temperature has a profound influence on the extent of crack healing and the degree of strength recovery. The optimum heat‐treatment temperature was 1100 ℃ for one hour at an atmospheric level. In the two kinds of solutions, the cracks in a specimen were reduced with increasing time, and the surface of the crack healed specimen had a greater number of black and white spots. The strength of the corroded cracked specimen was similar to that of the cracked specimen. The strength of the corroded crack healed specimen decreased 47% and 75% compared to that of the crack healed specimen in the acid and alkaline solutions, respectively. Therefore, the corrosion of SiC ceramics is faster in an alkaline solution than in an acid solution.

참고문헌 (15)

  1. Ando, K., "A Preliminary Study on Crack Healing Behavior of Si3N4", SiC Composite Cermiacs, 1998, pp.21, 119~122
  2. Giancarli, L., "Design Requirements for SiC : SiC Composites Structural Material in Fusion Power Reactor Blankets", Fusion Engineering and Design, 41, pp.65~171 (1998)
  3. Lee, S. K., "Crackhealing Behavior and Resultant Strength Poperties of Silicon Carbide Ceramic", Journal of the European Ceramic Society, 25, pp.569~576 (2005)
  4. 남기우, "SiC", SiC 복합재료 세라믹스 표면균열 탐지를 위한 초음파법 적용에 관한 기초연구, 2009, pp.29(5), 479~484[DOI]
  5. Kim, J. S., "Critical crack size of healing possibility of SiC ceramics", MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 527, pp.3236~3239 (2010), ELSEVIER SCIENCE SA
  6. Nam, K. W., "The High Temperature Strength of SiC Ceramics Based on SiO2 Nanocolloidal Employed", Materials Science and Engineering A, 527, pp.5400~5404 (2010)
  7. Nam, K. W., "Crack-Healing Behavior and Bending Strength Properties of SiC Ceramics Based on the Type of Additive SiO2 Employed", International Journal of Modern Physics B, 24, pp.2869~2874 (2010)
  8. Nam, K. W., "Application of Untrasonic Inspection to Characterization of Advanced SiC", SiC Composites, 2011, pp.417, 353~355
  9. Ki Woo Nam, "A fundamental study for the crack healing of SiC ceramics and SiCf", SiC composite ceramics, 2011, pp.12(6), 646~649[DOI]
  10. Raffray, A. R., "Design and Material Issues for High Performance SiCf", SiC-based Fusion Cower Cores, 2001, pp.55, 55~95
  11. Saddow, S. E., "Advances in Silicon Carbide Processing and Applications" (2004), Artech House, Inc.
  12. Sembokuya, H., "Corrosion Behavior of Alumina or Silicon Carbide Filled Epoxy Resin Immersed in Alkaline Solution"", Journal of Network Polymer(Japan), 23, pp.72~80 (2002)
  13. Snead, L. L., "Status of Silicon Carbide Composites for fFsion", J. Nucl. Mater., 233-237, pp.26~36 (1996)
  14. Sydow, U., "Electrochemical Corrosion of Silicon Carbide Ceramics. Pt.1: Electrochemical Investigation of Sintered Silicon Carbide (SSiC)", Materials and Corrosion, 61, pp.S.657~S.664 (2010)
  15. Takahashi, K., "Threshold Stress for Crack Healing of Mullite Reinforced by SiC Whiskers and SiC Particles and Resultant Fatigue Strength at the Healing Temperature", J. Am. Ceram. Soc., 90, pp.2159~2164 (2007)

관련 논문AI추천

이 간행물의 다른 논문 (15건)