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GC/ECD 및 GC/MS를 이용한 토양 중 PCBs 분석방법 고찰

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참고문헌

주제분류화학

초록

Abstract

This study was investigated both the Korean oficial soil test method and the international variousmethods for PCBs in soil sample. The analytical guideline of PCBs in contaminated soil were proposed basedon the official soil test methods by discussing the extraction, column cleanup, instrumental conditions, quantificationmethods of peak matching and individual isomers. The total 28 soil samples were selected by consideration ofECD) and gas chromatography/mass spectrometry(GC/MS). In this study, the PCBs were not detected as peakmatching method using GC/ECD, but PCBs detected 0.002~0.487 g/kg using GC/MS in backgroundconcentrations.

참고문헌 (12)

  1. 국립환경연구원, "폴리염화비페닐류 (PCBs)함유 폐기물의 적정관리방안에 관한 연구" (2003), 국립환경연구원
  2. M. D. Erickon, "Analytical Chemistry of PCBs" (1997), LewisPublishers
  3. 국립환경과학원, "절연유 중 폴리염화비페닐류 (PCBs)세부분석지침" (2004), 국립환경과학원
  4. 환경부, "토양오염공정시험방법" (2002), 환경부
  5. "Chlorinated biphenyl congeners in water, soil, sediment, and tissue by HRGC", HRMS, 1999, ~
  6. "일본 JIS방법" (2001)
  7. 환경부, "폐기물공정시험방법" (2004), 환경부
  8. "Polychlorinated biphenyls (PCBs) by GC"
  9. "Insulating liquids-Contamination by polychlorinated biphenyls (PCBs)-Method of determination by capillary column gas chromatography" (1997)
  10. "Soil quality-Determination of organochlorine pesticides and polychlorinated biphenyls-Gas chromatographic method with electron capture detection" (2002)
  11. "産業廢棄勿分析マニユアル" (1997), 日本環境測定分析協會
  12. ぎようせい, "PCB 처리기술가이드북" (1999), ぎようせい

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