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Silica Gel Promoted Mild, Efficient and Inexpensive Protocol for the Preparation of 3,4-dihydropyrano[c]chromenes

T. S. R. Prasanna|K. Mohana Raju
대한화학회|2011.08|대한화학회지 (Journal of the Korean Chemical Society)|제55권 제4호|pp. 662-665

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참고문헌

키워드

Silica gelmalononitrile방향족 알데히드one pot three-component condensationaromatic aldehyde4-hydroxycoumarin.실리카젤one pot three-component 축합반응말론니트릴4-히드록시쿠마린
주제분류화학

초록

Highly efficient, three-component condensation of aromatic aldehyde, malononitrile and 4-hydroxycoumarin promoted by neat silica gel at room temperature is described. The method offers an excellent alternative to the synthesis of 3,4-dihydropyrano[c]chromenes. The reactions are fast and clean, and the products are obtained with good yield and purity.

Abstract

Highly efficient, three-component condensation of aromatic aldehyde, malononitrile and 4-hydroxycoumarin promoted by neat silica gel at room temperature is described. The method offers an excellent alternative to the synthesis of 3,4-dihydropyrano[c]chromenes. The reactions are fast and clean, and the products are obtained with good yield and purity.

참고문헌 (18)

  1. Zhu, J., (2005), Wiley-VCH
  2. Kappe, C. O., , Acc. Chem. Res, 33, pp.879~ (2000)
  3. Domling, A., , Angew. Chem., Int. Ed, 39, pp.3168~ (2000)
  4. Ugi, I., , J. Heteroclcl. Chem, 37, pp.647~ (2000)
  5. Bienayme, H., , Chem. Eur. J, 6, pp.3321~ (2000)
  6. Shestopalov, A. M., , Org. Lett, 4, pp.423~ (2002)
  7. Bagley, M. C., , Chem. Commun, pp.1682~ (2002)
  8. Dallinger, D., , Org. Lett, 5, pp.1205~ (2003)
  9. Bonsignore, L., , Eur. J. Med. Chem, 28, pp.517~ (1993)
  10. Konkoy, C. S., , Chem. Abstr. 2001, 134, pp.29313~ (2000)
  11. Abdolmohammadi, S., , Tetrahedron lett, 48, pp.3299~ (2007)
  12. Heravi, M. M., , Catal. Commun, 10, pp.272~ (2008)
  13. Khurana, J. M., , conditions. Tetrahedron lett, 50, pp.4125~ (2009)
  14. Kidwai, M., , Synth. Commun, 36, pp.2737~ (2006)
  15. Shaker, R. M., , Pharmazie, 51, pp.148~ (1996)
  16. Wipf, P., , Org Lett, 6(20), pp.3593~ (2004)
  17. You, L., , Tetrahedron lett, 49, pp.5147~ (2008)
  18. Ahmadi, E., , Tetrahedron Lett, 48, pp.6954~ (2007)

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