Synthesis of Some 2-Amino-5-Substituted-1,3,4-Oxadiazoles Through the Electrooxidation of Semicarbazone
1
조회
0
다운로드
0
인용
0
참고문헌
키워드
초록
The synthesis of 2-amino-5-substituted-1,3,4-oxadiazoles 4 were carried out from the electrooxidation of semicarbazone 3 at the platinum electrode under controlled potential electrolysis in an undivided cell. This is an environmentally benign method in the field of synthetic organic chemistry. The non-aqueous solvents acetic acid and acetonitrile and a supporting electrolyte lithium perchlorate were used for the electrolysis in the electrooxidation. The products were structurally charecterised by IR, 1H-NMR, 13C-NMR and elemental analysis.
Abstract
The synthesis of 2-amino-5-substituted-1,3,4-oxadiazoles 4 were carried out from the electrooxidation of semicarbazone 3 at the platinum electrode under controlled potential electrolysis in an undivided cell. This is an environmentally benign method in the field of synthetic organic chemistry. The non-aqueous solvents acetic acid and acetonitrile and a supporting electrolyte lithium perchlorate were used for the electrolysis in the electrooxidation. The products were structurally charecterised by IR, 1H-NMR, 13C-NMR and elemental analysis.
참고문헌 (32)
- Holla, B. S, , Eur. J. Med. Chem, 35, pp.267~ (2000)
- Cesur, N, , Acta. Pharm. Turcica, 44, pp.23~ (2002)
- Laddi, U. V, , Indian J. Heterocycl. Chem, 11, pp.319~ (2002)
- Zou, X. Z, , J. Chem. Res. Synopses, 228 (2002)
- Zou, X. J, , J. Agric. Food Chem, 50, pp.3757~ (2002)
- Palaska, E, , Farmaco, 57, pp.101~ (2002)
- Tyagi, M, , Oriental. J. Chem, 18, pp.125~ (2002)
- Clapp, L. B, "Comprehensive Heterocyclic Chemistry", pp.365~ (1984), Pergamon Press
- Afiatpour, A, , Braz. J. Med. Biol. Res., 27, pp.1403~ (1994)
- Collins, T. J, "Green Chemistry Encyclopedia of Chemistry" (1997), 1997
- Anastas, P. T, "Green Chemistry: Theory and Practice" (1998), Oxford University Press
- Tundo, P, "Green Chemistry: Designing Chemistry for the Environment", pp.626~ (1996), ACS Sym
- Anastas, P. T, "Benign by Design: Alternative Synthetic Design for Pollution Prevention", pp.557~ (1994), ACS Sym
- Wilkinson, S. L, , Chem. Eng. News, 75, pp.35~ (1997)
- Anastas, P. T, , Critical Rev. Anal. Chem, 29, pp.167~ (1999)
- Tundo, P, "Green Chemistry: Challenging Perspectives" (2000), Oxford University Press
- Yadav, K. L, , Transactions of the SAEST, 40, pp.106~ (2005)
- Kumar, A, , Proc. Nat. Acad. Sci. India, 75A(4), pp.233~ (2005)
- Kumar, S, , J. Indian Chem. Soc., 82, pp.934~ (2005)
- Kumar, S, , Transactions of the SAEST, 41, pp.05~ (2006)
- Yadav, K. L, , J. Indian Chem. Soc., 81, pp.595~ (2004)
- Sharma, L. K, , Indian J Chem., Sec. B, 47, pp.1277~ (2008)
- Kumar, S, , J. Indian Chem. Soc, 83, pp.1160~ (2006)
- Sharma, L. K, , Transactions of the SAEST, 41, pp.48~ (2006)
- Yadav, K. L, , J Electrochem. Soc., 52(3), pp.114~ (2003)
- Hetzheim, A, , Adv. Heterocyclic Chem, 7, pp.183~ (1966)
- Hill, J, "In Com prehensive Heterocyclic Chemistry", pp.427~ (1984), Pergamon Press
- Gani, R. S, , Indian J. Heterocycl. Chem., 12, pp.25~ (2002)
- Golovlyova, S. M, , Chem. Heterocycl. Compd, 37, pp.1102~ (2001)
- Aboulwafa, O. M, , Sulfur Lett, 14, pp.181~ (1992)
- Faidallah, H. M, , Phos. Sulf. Sil. Rel. Elem., 67, pp.177~ (2002)
- Cappo, F. T, , Tetrahedron Lett, 45, pp.3257~ (2004)