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New Synthesis of Perhydrotriazolotriazoles Catalyzed by TiCl₄ under Ambient Conditions

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초록

Aromatic 2,3-diazabuta-1,3-dienes in glacial acetic acid with isothiocyanate in the presence of catalyst TiCl4at room temperature produced via criss-cross cycloaddition reactions the corresponding perhydro[1,2,4]triazolo[1,2-a][1,2,4]triazole-1,5-dithiones in relatively high yields and short reaction time.

Abstract

Aromatic 2,3-diazabuta-1,3-dienes in glacial acetic acid with isothiocyanate in the presence of catalyst TiCl4at room temperature produced via criss-cross cycloaddition reactions the corresponding perhydro[1,2,4]triazolo[1,2-a][1,2,4]triazole-1,5-dithiones in relatively high yields and short reaction time.

참고문헌 (20)

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