Effect of irradiation temperature on the nanoindentation behavior of P92 steel with thermomechanical treatment
1
조회
0
다운로드
0
인용
0
참고문헌
키워드
초록
The nanoindentation behavior of P92 steel with thermomechanical treatment under 3.5 MeV Fe13þ ion irradiation at room temperature, 400 and 700 C was investigated. Pop-in behavior is observed for all the samples with and without irradiation at room temperature, while the temperature dependence of pop-in behavior is only observed in irradiated samples. The average load and penetration depth at the onset of pop-in increase as the irradiation temperature increases, in line with the results of the maximum shear stress. Irradiation induced hardening is exhibited for all irradiated samples, but there is a significant reduction in the hardness of sample irradiated at 700 C in comparison to the samples irradiated at room temperature and 400 C. The ratio of hardness to elastic modulus for all samples decreases with increasing penetration depth except for samples at 700 C. With the increasing of irradiation temperature, the ratio of the irreversible work to the total work gradually decreases. In contrast, it increases for samples without irradiation
Abstract
The nanoindentation behavior of P92 steel with thermomechanical treatment under 3.5 MeV Fe13þ ion irradiation at room temperature, 400 and 700 C was investigated. Pop-in behavior is observed for all the samples with and without irradiation at room temperature, while the temperature dependence of pop-in behavior is only observed in irradiated samples. The average load and penetration depth at the onset of pop-in increase as the irradiation temperature increases, in line with the results of the maximum shear stress. Irradiation induced hardening is exhibited for all irradiated samples, but there is a significant reduction in the hardness of sample irradiated at 700 C in comparison to the samples irradiated at room temperature and 400 C. The ratio of hardness to elastic modulus for all samples decreases with increasing penetration depth except for samples at 700 C. With the increasing of irradiation temperature, the ratio of the irreversible work to the total work gradually decreases. In contrast, it increases for samples without irradiation
참고문헌 (63)
- C. Cabet, "Ferritic-martensitic steels for fission and fusion applications", J. Nucl. Mater, 523, pp.510~537 (2019)[DOI]
- L. Chen, "Microstructures and high-temperature mechanical properties of a martensitic heat-resistant stainless steel 403Nb processed by thermo-mechanical treatment", Metall. Mater. Trans, 45, pp.1498~1507 (2014)[DOI]
- S. Li, "Effect of thermo-mechanical treatment on microstructure and mechanical properties of P92 heat resistant steel", Mater. Sci. Eng, 559, pp.882~888 (2013)[DOI]
- M. Song, "A roadmap for tailoring the strength and ductility of ferritic", martensitic T91 steel via thermo-mechanical treatment, 2016, pp.112, 361~377
- S. Hollner, "High-temperature mechanical properties improvement on modified 9Cre1Mo martensitic steel through thermomechanical treatments", J. Nucl. Mater, 405, pp.101~108 (2010)[DOI]
- I. Yu Litovchenko, "The effect of heat treatment on the microstructure and mechanical properties of heat-resistant ferriticemartensitic steel EK-181", J. Nucl. Mater, 455, pp.665~668 (2014)[DOI]
- N. A. Polekhina, "Effect of high-temperature thermomechanical treatment in the austenite region on microstructure and mechanical properties of low-activated 12% chromium ferritic-martensitic steel EK-181", Tech. Phys, 62, pp.736~740 (2017)[DOI]
- A. Di Schino, "Effect of thermo-mechanical parameters on the mechanical properties of Eurofer97 steel for nuclear applications", Open Eng, 8, pp.349~353 (2018)[DOI]
- L. Tan, "Effects of alloying elements and thermomechanical treatment on 9Cr Reduced Activation FerriticeMartensitic(RAFM)steels", J. Nucl. Mater, 442, pp.S13~ (2013)[DOI]
- E. Little, "Influence of thermomechanical treatment on irradiation microstructures in an ODS ferritic steel", Effects of Radiation on Materials: 17th International Symposium (1996), ASTM International
- G. S. Was, "Emulation of reactor irradiation damage using ion beams", Scripta Mater, 88, pp.33~36 (2014)[DOI]
- D. L. Krumwiede, "Direct comparison of nanoindentation and tensile test results on reactor-irradiated materials", J. Nucl. Mater, 504, pp.135~143 (2018)[DOI]
- C. Heintze, "Ionirradiation-induced damage of steels characterized by means of nanoindentation", Nucl. Instrum. Methods Phys. Res. Sect. B Beam Interact. Mater. Atoms, 267, pp.1505~1508 (2009)[DOI]
- Bingsheng Li, "Evaluation of helium effect on irradiation hardening in F82H, ODS, SIMP and T91 steels by nano-indentation method", Fusion Engineering and Design, 142, pp.6~12 (2019), Elsevier BV[DOI]
- A. A. Nikitin, "Nanoindentation Study of the Effect of Low-Temperature Ion Irradiation on the Hardness of a Ferritic–Martensitic EK-181 Steel", Russian Metallurgy (Metally), 2019(11), pp.1184~1189 (2019), Pleiades Publishing Ltd[DOI]
- L. Tan, "Microstructural stability of tantalum-alloyed ferritic-martensitic steel with neutron irradiation to 7. 4 dpa at~490"C", Materialia, 9, pp.100608~ (2020)[DOI]
- Qingshan Li, "Irradiation-Induced Hardening and Softening of CLAM Steel Under Fe Ion Irradiation", Metals and Materials International, 23(6), pp.1106~1111 (2017), 대한금속·재료학회[DOI]
- H. Yan, "Early-stage microstructural evolution and phase stability in neutron-irradiated ferritic-martensitic steel T91", J. Nucl. Mater, 557, pp.153207~ (2021)[DOI]
- H. Ogiwara, "Irradiation-induced hardening mechanism of ion irradiated JLF-1 to high fluences", Fusion Eng. Des, 81, pp.1091~1097 (2006)[DOI]
- M. Rieth, "Technological aspects in blanket design : effects of microalloying and thermo-mechanical treatments of EUROFER97 type steels after neutron irradiation", Fusion Eng. Des, 168, pp.112645~ (2021)[DOI]
- Anders Bäcklin, "Treatise on Heavy-Ion Science", Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, 252(1), pp.128~ (1986), Elsevier BV[DOI]
- W. C. Oliver, "An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments", J. Mater. Res, 7, pp.1564~1583 (1992)[DOI]
- F. P€ohl, "Pop-in behavior and elastic-to-plastic transition of polycrystalline pure iron during sharp nanoindentation", Sci. Rep, 9, pp.1~12 (2019)[DOI]
- T. G. N. C. Zhu, "Incipient plasticity and dislocation nucleation of FeCoCrNiMn high-entropy alloy", Acta Mater, 61, pp.2993~3001 (2013)[DOI]
- T. Ohmura, "Nanoindentation-induced deformation behavior in the vicinity of single grain boundary of interstitial-free steel", Mater. Trans, 46, pp.2026~2029 (2005)[DOI]
- K.L. Johnson, "Contact Mechanics", Nanoindentation of Brittle Solids, pp.1~2 (2014), CRC Press[DOI]
- W. Jiang, "Creep damage and crack initiation in P92-BNi2 brazed joint", Mater. Des, 72, pp.63~71 (2015)[DOI]
- G. M. P. W. C. Oliver, "Measurement of hardness and elastic modulus by instrumented indentation : advances in understanding and refinements to methodology", J. Mater. Res, 19, pp.3~20 (2004)[DOI]
- A. Montagne, "Influence of pre-existing dislocations on the pop-in phenomenon during nanoindentation in MgO", Acta Mater, 61, pp.4778~4786 (2013)[DOI]
- L. Tan, "Microstructural evolution of neutron-irradiated T91 and NF616 to~4. 3 dpa at 469"C", J. Nucl. Mater, 493, pp.12~20 (2017)[DOI]
- P. P. Liu, "A model to evaluate the nano-indentation hardness of ion-irradiated materials", Nucl. Instrum. Methods Phys. Res. Sect. B Beam Interact. Mater. Atoms, 342, pp.13~18 (2015)[DOI]
- I. Manika, "Effect of substrate hardness and film structure on indentation depth criteria for film hardness testing", J. Phys. Appl. Phys, 41, pp.074010~ (2008)[DOI]
- X. Zhao, "Determination of mechanical properties of thermally grown oxide on Fecralloy by nano-indentation", Thin Solid Films, 515, pp.8393~8401 (2007)[DOI]
- M. Lei, "Micro-mechanics of nanostructured carbon", shape memory polymer hybrid thin film, 2016, pp.12, 106~114
- Yang-Tse Cheng, "Relationships between hardness, elastic modulus, and the work of indentation", Applied Physics Letters, 73(5), pp.614~616 (1998), AIP Publishing[DOI]
- Z. Xu, "Precipitate phases in ferritic", martensitic steel P92 after thermomechanical treatment, 2018, pp.509, 355~365
- R Schäublin, "Differences in the microstructure of the F82H ferritic", martensitic steel after proton and neutron irradiation, 2000, pp.283-287, 339~343[DOI]
- D. F. Bahr, "Non-linear deformation mechanisms during nanoindentation", Acta Mater, 46, pp.3605~3617 (1998)[DOI]
- Z. Wang, "Influences of surface preparation on nanoindentation pop-in in single-crystal Mo", Scripta Mater, 65, pp.469~472 (2011)[DOI]
- J. Lian, "Grain size and grain boundary effects on the mechanical behavior of fully stabilized zirconia investigated by nanoindentation", Scripta Mater, 56, pp.1095~1098 (2007)[DOI]
- A. Gouldstone, "Nanoindentation : simulation of defect nucleation in a crystal", Nature, 11, pp.656~ (2001)[DOI]
- J. E. Bradby, "Pop-in events induced by spherical indentation in compound semiconductors", J. Mater. Res, 19, pp.380~386 (2004)[DOI]
- Y. Gao, "Strength statistics of single crystals and metallic glasses under small stressed volumes", Prog. Mater. Sci, 82, pp.118~150 (2016)[DOI]
- H Iwakiri, "Hardening behavior of molybdenum by low energy He and D ion irradiation", Journal of Nuclear Materials, 258-263, pp.873~878 (1998), Elsevier BV[DOI]
- K. Jin, "Quantifying early stage irradiation damage from nanoindentation pop-in tests", Scripta Mater, 157, pp.49~53 (2018)[DOI]
- E. Kuramoto, "Positron annihilation lifetime measurement of irradiated stainless steels", Journal of Nuclear Materials, 133-134, pp.561~565 (1985), Elsevier BV[DOI]
- M. G€oken, "Pop-ins in nanoindentations-the initial yield point", Zeitschrift Fuer Metallkunde, 2001, pp.92, 1061~
- T. F. Page, "The deformation behavior of ceramic crystals subjected to very low load(nano)indentations", J. Mater. Res, 7, pp.450~473 (1992)[DOI]
- T. Yang, "Effects of temperature on the irradiation responses of Al0. 1CoCrFeNi high entropy alloy", Scripta Mater, 144, pp.31~35 (2018)[DOI]
- M. A. Lodes, "Influence of dislocation density on the pop-in behavior and indentation size effect in CaF2 single crystals : experiments and molecular dynamics simulations", Acta Mater, 59, pp.4264~4273 (2011)[DOI]
- T. H. Ahn, "Relationship between yield point phenomena and the nanoindentation pop-in behavior of steel", J. Mater. Res, 7, pp.39~44 (2012)[DOI]
- X. Xiao, "Comparison of linear and square superposition hardening models for the surface nanoindentation of ion-irradiated materials", J. Nucl. Mater, 503, pp.110~115 (2018)[DOI]
- C. Sun, "chemistry and mechanical properties of Ni-based superalloy Rene N4 under irradiation at room temperature", Acta Mater, 95, pp.357~365 (2015)[DOI]
- J.J. Shi, "Characterization of proton-irradiated Chinese A508-3-type reactor pressure vessel steel by slow positron beam, TEM, and nanoindentation", Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, 443, pp.62~69 (2019), Elsevier BV[DOI]
- G. Gupta, "Microstructural evolution of proton irradiated T91", J. Nucl. Mater, 351, pp.162~173 (2006)[DOI]
- H. Tanigawa, "Irradiation effects on precipitation in reduced-activation ferritic", martensitic steels, 2005, pp.46, 469~474
- Z. Yang, "Dissolution of M23C6 and new phase re-precipitation in Fe ion-irradiated RAFM steel", Metals, 8, pp.349~ (2018)[DOI]
- S. Kano, "Instability of MX and M23C6 type precipitates in F82H steels under 2. 8 MeV Fe2þ irradiation at 673 K", Nucl. Mater. Energy, 17, pp.56~61 (2018)[DOI]
- C. Heintze, "Ion-irradiation-induced damage in FeeCr alloys characterized by nanoindentation", J. Nucl. Mater, 417, pp.980~983 (2011)[DOI]
- Jun Zhu, "The Effect of Fe-Ion Irradiation on Hardness Changes in P92 Ferritic", Martensitic Steel, 2013, pp.446-447, 418~421[DOI]
- D. R. H. R. L. Klueh, "High-Chromium Ferritic and Martensitic Steels for Nuclear Applications", ASTM International, ~ (2001)
- G. S. Was, "Fundamentals of Radiation Materials Science" (2007), Springer Berlin Heidelberg
- Y. -T. Cheng, "Relationships between hardness, elastic modulus, and the work of indentation", Appl. Phys. Lett, 73, pp.614~616 (1998)[DOI]
