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정확한 위상정보를 얻기 위한 탈초점 영상들의 이미지 처리기법

Image Processing of Defocus Series TEM Images for Extracting Reliable Phase Information

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초록

We discuss the experimental procedure for extracting reliable phase information from a defocus series of transmission electron microscopy (TEM) dark-field images using the transport of intensity equation (TIE). Taking InGaN/GaN multi-quantum well light-emitting diode as a model system, various factors affecting the final result of reconstructed phase such as TEM sample preparation, TEM imaging condition, image alignment, the correction of defocus values and the use of high frequency pass filter are evaluated. The obtained phase of wave function was converted to the geometric phase of the corresponding lattice planes,which was then used for the two-dimensional mapping of lattice strain following the dark-field inline holography (DIH) routine. The strain map obtained by DIH after optimized image processing is compared with that obtained by the geometric phase analysis of high resolution TEM (HRTEM) image, manifesting that DIH yields more accurate and reliable strain information than HRTEM-based GPA.

Abstract

We discuss the experimental procedure for extracting reliable phase information from a defocus series of transmission electron microscopy (TEM) dark-field images using the transport of intensity equation (TIE). Taking InGaN/GaN multi-quantum well light-emitting diode as a model system, various factors affecting the final result of reconstructed phase such as TEM sample preparation, TEM imaging condition, image alignment, the correction of defocus values and the use of high frequency pass filter are evaluated. The obtained phase of wave function was converted to the geometric phase of the corresponding lattice planes,which was then used for the two-dimensional mapping of lattice strain following the dark-field inline holography (DIH) routine. The strain map obtained by DIH after optimized image processing is compared with that obtained by the geometric phase analysis of high resolution TEM (HRTEM) image, manifesting that DIH yields more accurate and reliable strain information than HRTEM-based GPA.

참고문헌 (17)

  1. Allen LJ, "Exit wave reconstruction at atomic resolution", Ultramicroscopy, 100, pp.91~104 (2004)
  2. Allen LJ, "Electron microscope Cs correction using iterative wave-function reconstruction", Microscopy and Analysis, 52, pp.5~7 (2006)
  3. Carbone L, "Synthesis and micrometer-scale assembly of colloidal CdSe", CdS nanorods prepared by a seeded growth approach, 2007, pp.7, 2942~2950
  4. Chang LY, "Comparisons of linear and nonlinear image restoration", Microsc Microanal, 12, pp.469~475 (2006)
  5. Coene WMJ, "Phase retrieval through focus variation for ultra-resolution in field emission transmission microscopy", Phys Rev Lett, 69, pp.3743~3746 (1992)
  6. Coene WMJ, "Maximumlikelihood method for focus-variation image reconstruction in high resolution transmission microscopy", Ultramicroscopy, 64, pp.109~135 (1996)
  7. Hÿtch MJ, "Nanoscale holographic interferometry for strain measurements in electronic devices", Nature, 453, pp.1086~1090 (2008)
  8. Hÿtch MJ, "Quantitative measurement of displacement and strain fields from HREM micrographs", Ultramicroscopy, 74, pp.131~146 (1998)
  9. Ishizuka K, "Phase measurement of atomic resolution image using transport of intensity equation", J Elec Micro, 54(3), pp.191~197 (2005)
  10. Jonhson CL, "Effects of elastic anisotropy on strain distributions in decahedral gold nanoparticles", Nature Materials, 7, pp.120~124 (2008)
  11. Koch CT, "A flux-preserving non-linear inline holography reconstruction algorithm for partially coherent electrons", Ultramicroscopy, 108, pp.141~150 (2008)
  12. Koch CT, "An efficient, simple, and precise way to map strain with nanometer resolution in semiconductor devices", Appl Phys Lett, 96 (2010)
  13. Koch CT, "SESAM: Exploring the frontiers of electron microscopy", Microsc Microanal, 12, pp.506~514 (2006)
  14. Mitome M, "Quantitativeness of phase measurement by transport of intensity equation", J Elec Micro, 59(1), pp.33~41 (2010)
  15. Özdöl VB, "A non damaging electron microscopy approach to map In distribution in InGaN light-emitting diodes", J Appl Phys, 108 (2010)
  16. Taraci JL, "Strain mapping in nanowires", Nanotechnology, 16, pp.2365~2371 (2005)
  17. Teague MR, "Deterministic phase retrieval: a Green’s function solution", J Opt Soc Am, 73, pp.1434~1441 (1983)

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