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Effect of composition on the ability to form SiC/SiO2-C composite from rice husk and silica gel

Tran Van Khai|Kieu Do Trung Kien|Nguyen Vu Uyen Nhi|Huynh Ngoc Minh|Do Quang Minh
청정에너지연구소 (Clean-Energy Research Institute)|2021.04|Journal of Ceramic Processing Research|제22권 제2호|pp. 246-251|DOI 10.36410/jcpr.2021.22.2.246

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키워드

Silicon carbiderice huskSiC/SiO2-C composite
주제분류재료공학

초록

Rice husk is a waste product of agricultural production of rice. Every year, the agricultural production of Vietnam emits about10 million tons of rice husks. Rice husks are usually treated by burning method or discharged into rivers, causing manynegative impacts on the environment. In this study, the rice husk/silica gel ratio components were investigated to form SiC/SiO2-C composite in a CO2 environment at 1000 oC for 60 min. The products after pyrolysis were determined SiC, SiO2, andfree C contents according to ISO 21068-2: 2008 standards. The functional groups and mineral composition of composites wereanalyzed by Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). The microstructure and elementdistribution of them were observed by scanning electron microscope (SEM) and Energy-dispersive X-ray (EDX) mapping. Theresults showed that the optimum rice husk/silica gel ratio to form SiC/SiO2-C was 1.4/1. The sample after pyrolysis hadchemical composition including 14% SiC, 63% SiO2, 23% free C (%wt.) and the phase composition including amorphouscarbon, β-SiC, 6H-SiC, 4H-SiC, cristobalite. Composite SiC/SiO2-C can apply to advanced friction systems. This can be seenas an effective method to treat rice husk waste and improved the economic value of rice plants.

Abstract

Rice husk is a waste product of agricultural production of rice. Every year, the agricultural production of Vietnam emits about10 million tons of rice husks. Rice husks are usually treated by burning method or discharged into rivers, causing manynegative impacts on the environment. In this study, the rice husk/silica gel ratio components were investigated to form SiC/SiO2-C composite in a CO2 environment at 1000 oC for 60 min. The products after pyrolysis were determined SiC, SiO2, andfree C contents according to ISO 21068-2: 2008 standards. The functional groups and mineral composition of composites wereanalyzed by Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). The microstructure and elementdistribution of them were observed by scanning electron microscope (SEM) and Energy-dispersive X-ray (EDX) mapping. Theresults showed that the optimum rice husk/silica gel ratio to form SiC/SiO2-C was 1.4/1. The sample after pyrolysis hadchemical composition including 14% SiC, 63% SiO2, 23% free C (%wt.) and the phase composition including amorphouscarbon, β-SiC, 6H-SiC, 4H-SiC, cristobalite. Composite SiC/SiO2-C can apply to advanced friction systems. This can be seenas an effective method to treat rice husk waste and improved the economic value of rice plants.

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