Temperature-dependent ferroelectric and piezoelectric response of Yb3+ and Tm3+ co-doped Ba0.95Ca0.05Ti0.90Zr0.10O3 lead-free ceramic
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The electrical properties of piezoelectric ceramics are temperature-dependent, which affects their potential for applications inenvironments with temperature variation. In this work, Yb3+ and Tm3+ co-doped Ba0.95Ca0.05Ti0.90Zr0.10O3 (BCTZ-YT) denselead-free ceramic was prepared using a modified polymeric precursor route. On the basis of structural and electricalmeasurements at various temperatures, the mechanism of a lack of oxygen vacancies, small structural defects, and small defectdipoles was deduced. This study reveals that the ferroelectricity and piezoelectricity are temperature-dependent, whereas thecapacitance is essentially unchanged with increasing temperature owing to the presence of a pure orthorhombic phase. Thecapacitance of the BCTZ-YT ceramic was essentially constant at ~4.5 nF, the thermal expansion coefficient was 8.57 × 10−6 K−1below 75 oC, and the piezoelectric response (d33*) was above 416 pm/V in a wide temperature range (-20 to 40 oC), suggestingthe results of this study are expected to inform future research.
Abstract
The electrical properties of piezoelectric ceramics are temperature-dependent, which affects their potential for applications inenvironments with temperature variation. In this work, Yb3+ and Tm3+ co-doped Ba0.95Ca0.05Ti0.90Zr0.10O3 (BCTZ-YT) denselead-free ceramic was prepared using a modified polymeric precursor route. On the basis of structural and electricalmeasurements at various temperatures, the mechanism of a lack of oxygen vacancies, small structural defects, and small defectdipoles was deduced. This study reveals that the ferroelectricity and piezoelectricity are temperature-dependent, whereas thecapacitance is essentially unchanged with increasing temperature owing to the presence of a pure orthorhombic phase. Thecapacitance of the BCTZ-YT ceramic was essentially constant at ~4.5 nF, the thermal expansion coefficient was 8.57 × 10−6 K−1below 75 oC, and the piezoelectric response (d33*) was above 416 pm/V in a wide temperature range (-20 to 40 oC), suggestingthe results of this study are expected to inform future research.
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