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Investigation of nanostructures LiZnCu ferrite by auto combustion method

Emad K. Al-Shakarchi|Saad Shakir Hussein
청정에너지연구소 (Clean-Energy Research Institute)|2024.06|Journal of Ceramic Processing Research|제25권 제3호|pp. 323-331|DOI 10.36410/jcpr.2024.25.3.323

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키워드

Spinel structureAuto-combustion methodNanostructure ferritesScherrer method.
주제분류재료공학

초록

A nanostructure of Lithium-Zinc-Copper ferrite (LiZnCu-Ferrite) prepared experimentally by the auto-combustion methoddepends on different parameters. The auto-combustion method was operated at temperature (160 °C), which is suitable toprepare the required nanostructure ferrite phase. The dependent composition was [Li0.5-xZnxCuxFe2.5-xO4 at (x=0, 0.05, 0.15,0.25, 0.35, and 0.45)]. A pre-firing at temperature (650 °C) was applied during the calcination process that was suitable toremove unwanted products. The sintering at temperature (800 °C) was suitable for a pelletized shape of ferrite samples. The X-ray diffraction (XRD) pattern showed a spinel structure of ferrite phase produced for all samples under study withthe lattice constant in the range (8.345-8.368 Å) as a function of different (x). The crystallite size was in the range (18.41-30.27nm) calculated by the Scherrer method. The transmission electron microscope (TEM) showed a production of nanorod inthe size range (10-45 nm), and nanoparticles in the size range (10-40 nm). There is a coincidence between the results ofXRD and TEM analysis. On the other hand, the scanning electron microscope (SEM) showed the surface morphology andthe nature of grain size, which is a sign on the presence of nanostructure. It was agreed with the XRD analysis preparedin ferromagnetic materials.

Abstract

A nanostructure of Lithium-Zinc-Copper ferrite (LiZnCu-Ferrite) prepared experimentally by the auto-combustion methoddepends on different parameters. The auto-combustion method was operated at temperature (160 °C), which is suitable toprepare the required nanostructure ferrite phase. The dependent composition was [Li0.5-xZnxCuxFe2.5-xO4 at (x=0, 0.05, 0.15,0.25, 0.35, and 0.45)]. A pre-firing at temperature (650 °C) was applied during the calcination process that was suitable toremove unwanted products. The sintering at temperature (800 °C) was suitable for a pelletized shape of ferrite samples. The X-ray diffraction (XRD) pattern showed a spinel structure of ferrite phase produced for all samples under study withthe lattice constant in the range (8.345-8.368 Å) as a function of different (x). The crystallite size was in the range (18.41-30.27nm) calculated by the Scherrer method. The transmission electron microscope (TEM) showed a production of nanorod inthe size range (10-45 nm), and nanoparticles in the size range (10-40 nm). There is a coincidence between the results ofXRD and TEM analysis. On the other hand, the scanning electron microscope (SEM) showed the surface morphology andthe nature of grain size, which is a sign on the presence of nanostructure. It was agreed with the XRD analysis preparedin ferromagnetic materials.

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