분광분석법을 이용한 수종 MTA의 치관변색 평가
Spectrophotometric Analysis of Crown Discoloration Induced by Various MTA Based Materials
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Mineral trioxide aggreagate는 치수 치료제로서 많이 사용되고 있는 재료중 하나이다. 그 중 가장 널리 쓰이고 있는Proroot white MTA는 치아 변색을 일으킨다는 단점이 있다. 이번 연구에서는 MTA 기반 재료들인 Proroot wMTA, Biodentine, Endocem, RetroMTA를 치수강에 각각 채워넣어 시간에 따른 치경부의 변색을 비교하고자 하였다. 교정적인 이유로 발치된 75개의 소구치를 사용하여 무작위로 4개의 실험군(n = 60)과 한 개의 대조군(n = 15)으로 나누었다. 치아는 CEJ 하방 2 mm로 수평절단 하였다. 각각의 재료들을 제조사의 지시에 따라 준비한 후 치수강에 채워넣고입구를 레진을 이용하여 봉인하였다. 치아 색조 측정은 국제조명위원회(Commission International de I’Eclairage, CIE) 의 CIE L*a*b* system을 사용하였다. 색조는 분광 광도계를 사용하여 재료를 넣기 전, 재료를 넣고 1일, 1주, 2주, 4주, 8 주, 12주, 16주 후로 총 8번 측정하였다. 이원 변량 분산분석(Two way repeated ANOVA)을 사용하여 시간에 따른 CIE L*, a*, b*와 ΔE값을 비교 평가하였고 실험군과 대조군과의 통계적 유의성과 상호관계는 본페로니 검정으로 사후 검정하여p 값이 0.05이하일 때 통계학적으로 유의하다고 간주하였다. Proroot wMTA는 시간에 따라 계속적인 L*값의 감소를 보였고, Endocem은 재료를 넣은 직 후 육안으로 인지 불가능한 약간의 회색조 변색을 보였으며, Biodentine과 RetroMTA는 상대적으로 다른 재료보다 색 안정성을 보였다. 결론적으로, 방사선 불투과성 물질로서 산화 비스무스가 포함된 Proroot wMTA와 Endocem은 치관 변색을 보인 반면, 방사선 불투과성 물질로서 산화 지르코늄이 포함된 Biodentine과 RetroMTA는 시간에 따른 유의한 색 변화를 보이지 않았다.
Abstract
Mineral trioxide aggregate have been used for many years as a pulp therapy material. The most widely used product, Proroot white MTA has a major drawback that it causes tooth discoloration. This study assessed discoloration of crown when various MTA-based materials were placed in the coronal aspect of the root canal. Seventy-five single-rooted, unrestored premolar teeth were selected. The teeth were randomly assigned to four experimental groups, each of Biodentine, Proroot wMTA, Endocem, RetroMTA and one negative control groups. Color measurements were utilized by the Commission International de I’Eclairage’s L*a*b* system with spectrophotometer. The color was assessed eight times : initial, 1 day, 1 week, 2 weeks, 4 weeks, 8 weeks, 12 weeks, and 16 weeks after the placement. Statistical analysis was performed using the 2-way repeated analysis of variance and Bonferroni’s method with p < 0.05. Proroot wMTA induced significant decreases in L* values during experiment period. Tooth samples from the Endocem group presented indistinct grayish color changes. The Biodentine and RetroMTA showed color stability. Consequently, while Proroot wMTA and Endocem that contain bismuth oxide as a radiopacifier showed tooth discoloration, displayed no sign of discoloration Biodentine and RetroMTA that contain zirconium oxide as a radiopacifier.
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