수은 삼중점 온도 실현의 교정 기관 내 비교
Intralaboratory Comparison of the Realization of the Triple-point Temperature of Mercury
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An intralaboratory comparison of the realization of the triple-point temperature of mercury, which is defined as .38.8344℃ on the international temperature scale of 1990 (ITS-90), was conducted at the Korea Research Institute of Standards and Science (KRISS), the national metrology institute of Korea. To this end, four triple-point-of-mercury cells were compared using the resistance ratio measurementof a standard platinum resistance thermometer to validate the calibration results obtained using the triple-point-of-mercury cells at KRISS. The triple-point temperatures of all the four cells, one of which is designated as the national standard cell, were within 0.3mK of the national standard. Based on 13 experiments on the four triple-point-of-mercury cells, the uncertainty in the comparison of the triple-point-of-mercury cells was 0.08 mK, and the uncertainty in the realization of the triple-point temperature of mercury was 0.19mK. The results of the intralaboratory comparison validated that utilizing any of the four triple-point-of-mercury cells would result in the realization of a temperature within 0.3 mK of the average value determined by two key international comparisons for the realizationof .38.3844℃ following the ITS-90.
Abstract
An intralaboratory comparison of the realization of the triple-point temperature of mercury, which is defined as .38.8344℃ on the international temperature scale of 1990 (ITS-90), was conducted at the Korea Research Institute of Standards and Science (KRISS), the national metrology institute of Korea. To this end, four triple-point-of-mercury cells were compared using the resistance ratio measurementof a standard platinum resistance thermometer to validate the calibration results obtained using the triple-point-of-mercury cells at KRISS. The triple-point temperatures of all the four cells, one of which is designated as the national standard cell, were within 0.3mK of the national standard. Based on 13 experiments on the four triple-point-of-mercury cells, the uncertainty in the comparison of the triple-point-of-mercury cells was 0.08 mK, and the uncertainty in the realization of the triple-point temperature of mercury was 0.19mK. The results of the intralaboratory comparison validated that utilizing any of the four triple-point-of-mercury cells would result in the realization of a temperature within 0.3 mK of the average value determined by two key international comparisons for the realizationof .38.3844℃ following the ITS-90.
참고문헌 (10)
- H. Preston-Thomas, "The International Temperature Scale of 1990 (ITS-90)", Metrologia, 27(1), pp.3~10 (1990)
- B. W. Mangum, "Summary of comparison of realizations of the ITS90 over the range 83.8058 K to 993.473 K: CCT comparison CCT-K3", Metrologia, 39(2), pp.119~205 (2002)
- International Organization for Standardization, "General requirement for the competence of testing and calibration laboratories", ISO, 2017
- 감기술, "표준백금저항온도계를 이용한 온도측정능력 상호비교", 센서학회지, 18(1), pp.86~94 (2009), 한국센서학회
- K. H. Kang, "Realization of triple point of Ne, O2, Ar, Hg and H2O for international comparison of capsule-type platinum resistance thermometer", J. Sens. Sci. Technol, 9(3), pp.153~162 (2000)
- A. G. Steele, "CCT-K2: key comparison of capsule-type standard platinum resistance thermometers from 13.8 K to 273.16 K", Metrologia, 39(6), pp.551~571 (2002)
- 양인석, "국가표준향상과 핵심국제비교를 위한 물의 삼중점 온도 측정", 센서학회지, 30(5), pp.349~356 (2021), 한국센서학회
- Joint Committee for Guides in Metrology, "Evaluation of measurement data − Guides to the expression of uncertainty in measurement", JCGM, 100 (2008)
