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금속환원법에 의한 바나듐 분말 추출

Extraction of Vanadium Powder by Metallothermic Reduction

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키워드

주제분류금속공학

초록

The extraction of metallic pure vanadium powder from raw oxide has been tried by Mg-reduction. In first stage, V2O5 powders as initial raw material was reduced by hydrogen gas into V2O3 phase. V2O3 powder was reduced in next stage by magnesium gas at 1,073K for 24 hours. After reduction reaction, the MgO component mixed with reduced vanadium powder were dissolved and removed fully in 10% HCl solution for 5 hours at room temperature. The oxygen content and particle size of finally produced vanadium powders were 0.84 wt% and 1 μm, respectively.

Abstract

The extraction of metallic pure vanadium powder from raw oxide has been tried by Mg-reduction. In first stage, V2O5 powders as initial raw material was reduced by hydrogen gas into V2O3 phase. V2O3 powder was reduced in next stage by magnesium gas at 1,073K for 24 hours. After reduction reaction, the MgO component mixed with reduced vanadium powder were dissolved and removed fully in 10% HCl solution for 5 hours at room temperature. The oxygen content and particle size of finally produced vanadium powders were 0.84 wt% and 1 μm, respectively.

참고문헌 (11)

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  10. 이동원, "마그네슘환원에 의한 지르코늄-티타늄 합금분말 합성", 한국분말야금학회지, 18(4), pp.359~364 (2011), 한국분말야금학회

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