Synthesis of Nanosized Nickel Particle from Spent Cathodic Material Containing Lithium
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초록
Due to the rapid development of electricity, electronics, information communication, and biotechnology in recent years, studies are actively being conducted on nanopowders as it is required not only for high strengthening but also for high-function powder with electric, magnetic, and optical properties. Nonetheless, studies on nickel nanopowders are rare. In this study of the synthesis of nickel nanoparticles from LiNiO2 (LNO), which is a cathode active material, we have synthesized the nanosized nickel powder by the liquid reduction process of NiSO4 obtained through the leaching and purification of LNO. Moreover, we have studied the reduction reaction rate according to the temperature change of liquid phase reduction and the change of particle size as a function of NaOH addition amount using hydrazine monohydrate (N2H4·H2O) and NaOH.
Abstract
Due to the rapid development of electricity, electronics, information communication, and biotechnology in recent years, studies are actively being conducted on nanopowders as it is required not only for high strengthening but also for high-function powder with electric, magnetic, and optical properties. Nonetheless, studies on nickel nanopowders are rare. In this study of the synthesis of nickel nanoparticles from LiNiO2 (LNO), which is a cathode active material, we have synthesized the nanosized nickel powder by the liquid reduction process of NiSO4 obtained through the leaching and purification of LNO. Moreover, we have studied the reduction reaction rate according to the temperature change of liquid phase reduction and the change of particle size as a function of NaOH addition amount using hydrazine monohydrate (N2H4·H2O) and NaOH.
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