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전기방사를 이용한 S-Keratose / PVA 부직포의 제조

Preparation of S-keratose/PVA Nonwoven Webs by Electrospinning

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Abstract

keratose(S-keratose) could be obtained by oxidizing the wool keratin with performic acid. S-keratose/PVA solutions were made by dissolving them in the formic acid and S-keratose/PVA web of sub-micron size was made by electro-spinning technique. SEM, elemental analysis, FT-IR, X-ray diffractometry, and TGA were used to characterize the properties of S-keratose/PVA solutions and fibers. As the S-keratose content in S-keratose/PVA solution increased, viscosity of solution decreased while electrical conductivity has increased. The fiber diameter has decreased with increasing the S-keratose content. S-keratose/PVA ratio in fibers were similar to the ratio in the solutions. The crystalline structures of S-keratose and PVA existed separately in the electrospun webs. Thermal stability of the web increased with the PVA content increasing.

참고문헌 (11)

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  10. "The Effect of Processing Variables on the Morphology of Electrospun Nanofibers and Textiles", 42, pp.261~272 (2001)
  11. "The Infrared Spectra of Polypeptides in Various Conformations" (1961)

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