자초 분말 염료 제조를 위한 전처리 공정 연구
Pretreatment Process for Production of the Gromwell Colorants Powder
0
조회
0
다운로드
4
인용
0
참고문헌
키워드
초록
In this work, colorants extraction process from gromwell was studied for making powder form of colorants by solving the high viscosity problem of gromwell extracts. In order to do that, sugar extracted together with colorants must be pre-extracted. For sugar decomposition, gromwell roots were pretreated with various enzyme solutions. The total sugar content of pre-extract with enzyme solution was measured. Accordingly, the effects of enzyme type and pretreatment condition on sugar decomposition were investigated to find appropriate enzyme(amylase, hemicellulase, pectinase) and enzyme activity (100~1000unit), pre-extracted time(3~24hr). Color characteristics and dye uptake of dyed fabrics were evaluated. Gromwell colorants were assessed for their potential antimicrobial activities, which possibly expand their end use as functional pigments. The efficiency of removing sugar was increased in the order of hemicellulase, pectinase, amylase, H2O. Gromwell colorants powder yield was in the range of 4.4% to 9.8% depending on pretreatment enzyme. Gromwell colorants produced RP color on the silk and wool fabrics with good dye uptake. Antimicrobial activity of gromwell colorants will greatly increase its potentiality for applying as functional natural colorants in the future.
Abstract
In this work, colorants extraction process from gromwell was studied for making powder form of colorants by solving the high viscosity problem of gromwell extracts. In order to do that, sugar extracted together with colorants must be pre-extracted. For sugar decomposition, gromwell roots were pretreated with various enzyme solutions. The total sugar content of pre-extract with enzyme solution was measured. Accordingly, the effects of enzyme type and pretreatment condition on sugar decomposition were investigated to find appropriate enzyme(amylase, hemicellulase, pectinase) and enzyme activity (100~1000unit), pre-extracted time(3~24hr). Color characteristics and dye uptake of dyed fabrics were evaluated. Gromwell colorants were assessed for their potential antimicrobial activities, which possibly expand their end use as functional pigments. The efficiency of removing sugar was increased in the order of hemicellulase, pectinase, amylase, H2O. Gromwell colorants powder yield was in the range of 4.4% to 9.8% depending on pretreatment enzyme. Gromwell colorants produced RP color on the silk and wool fabrics with good dye uptake. Antimicrobial activity of gromwell colorants will greatly increase its potentiality for applying as functional natural colorants in the future.
참고문헌 (17)
- 남성우, "천연염료 분말 제조 및 날염", 한국염색가공학회지, 22(4), pp.314~324 (2010), 한국염색가공학회
- 김채연, "키토산과 천연색소를 이용한 Eco-Printing(제1보)", 한국염색가공학회지, 23(2), pp.90~99 (2011), 한국염색가공학회
- 신윤숙, "면직물에의 천연 인디고 염색 - 일단계 환원", 염색 공정 -, 2010, pp.22(2), 101~109[DOI]
- 조아랑, "석류 과피 추출물을 이용한 모발염색", 한국염색가공학회지, 20(6), pp.42~50 (2008), 한국염색가공학회
- 이광우, "오디 추출액을 이용한 상주실크의 천연염색", 한국염색가공학회지, 22(3), pp.207~213 (2010), 한국염색가공학회
- S. W. Nam, "Dyeing with Natural Dyes", Fiber Technology and Industry, 2(2), pp.238~257 (1998)
- H. Choi, "Analysis of Charactristics and Dyeing Properties of Gromwell Colornts (Part 1) - Components and Characteristics of Gromwell Colorants", J. Korean Society of Clothing and Textiles, 24(7), pp.1081~1087 (2000)
- A. Y. Park, "Color and Mordant Effect of Gallnut on Gromwell - Dyed Silk Fabrics", 석사, pp.2008
- 박영희, "자초 추출액을 이용한 염색직물의 항균성 및 소취성", 한국의류학회지, 27(1), pp.60~66 (2003), 한국의류학회
- J. H. Ju, "Progress on Phytochemical and Atopic Dermatitis-related Study of the Root of Lithospermum Erythrorhizon", J. Pharmacognosy, 41(2), pp.73~88 (2010)
- Y. L. Jang, "A Study on Dyeing according to pH and Mordant in Dyeing of Gromwell", 석사, pp.2010
- M. D. Bois, "Colorimetric Method for Determination of Sugars and Related Substances", Anal. Chem., 28(3), pp.350~356 (1956)
- A. K. Saha, "Determination of the Concentrations of Oligosaccharides, Complex Type Carbohydrates and Glycoproteins Using the Phenol- Sulfuric acid Method", Carbohydrate Research, 254(17), pp.157~167 (1994)
- T. Masuko, "Carbohydrate Analysis by a Phenol-Sulfuric acid Method in Microplate Format", Analytical Biochemistry, 339(1), pp.69~72 (2005)
- S. C. Choi, "Studies of Antimicrobial from Extracts of Impatiens Balsamina (Ⅰ), Textile Science and Engineering", J. Korean Fiber Society, 34(6), pp.393~399 (1997)
- S. Tanaka, "A Comparative Study on Anti-Inflammatory Activities of the Enantiomers, Shikonin and Alkannin", J. Nat. Prod., 49(3), pp.466~469 (1986)
